Rapid Library Synthesis of Amphiphiles Based On a Dioxinone Scaffold and Identification of Nonlamellar Liquid Crystals

Fuse Shinichiro; Nakamura Kentarou; Mifune Yuto; Marubayashi Hironori; Hijikuro Ichiro; Nojima Shuichi; Tanaka Hiroshi; Takahashi Takashi

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Rapid Library Synthesis of Amphiphiles Based On a Dioxinone Scaffold and Identification of Nonlamellar Liquid Crystals

机译：基于二恶英酮骨架的两亲物快速文库合成和非片状液晶的鉴定

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摘要

Linear and branched amphiphiles with different lengths of lipids and different numbers of hydroxyl groups were rapidly synthesized based on a dioxinone scaffold. The liquid crystalline (LC) properties of the synthesized amphiphiles in excess water were investigated by polarizing optical microscopy and small-angle X-ray scattering (SAXS) analysis. Novel -keto ester based amphiphiles that formed non-lamellar, inverted LC phases were identified.

机译：基于二恶英酮骨架，可以快速合成具有不同脂质长度和不同羟基数目的直链和支链两亲物。通过偏振光学显微镜和小角X射线散射（SAXS）分析研究了过量水中合成的两亲物的液晶（LC）特性。确定了新型的基于酮酯的两亲物，该两亲物形成了非薄片状的反相LC相。

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《Synlett》 |2014年第19期|共8页
作者
Fuse Shinichiro; Nakamura Kentarou; Mifune Yuto; Marubayashi Hironori; Hijikuro Ichiro; Nojima Shuichi; Tanaka Hiroshi; Takahashi Takashi;
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正文语种 eng
中图分类有机化学理论、物理有机化学;
关键词
multicomponent reaction; combinatorial chemistry; alkylation; nucleophilic addition; palladium;

机译：多组分反应;组合化学;烷基化;亲核加成;钯;

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1. Rapid Library Synthesis of Amphiphiles Based On a Dioxinone Scaffold and Identification of Nonlamellar Liquid Crystals [J] . Fuse Shinichiro, Nakamura Kentarou, Mifune Yuto, Synlett . 2014,第19期

机译：基于二恶英酮骨架的两亲物快速文库合成和非片状液晶的鉴定
2. Rapid and Structurally Diverse Synthesis of Multi-Substituted β-Keto Amide Derivatives Based on a Dioxinone Scaffold [J] . Shinichiro Fuse, Hayato Yoshida, Kazuya Oosumi, European journal of organic chemistry . 2014,第22期

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4. Synthesis of Gold Nanoparticles by Using a Bolaform Schiff Base Amphiphile at Liquid-Liquid interface [C] . Fengyan Wang, Tifeng Jiao International Conference on Mechatronics and Intelligent Materials . 2012

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Rapid Library Synthesis of Amphiphiles Based On a Dioxinone Scaffold and Identification of Nonlamellar Liquid Crystals

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