Synthesis of 1-azaxanthones by condensation of 1,3-bis(trimethylsilyloxy)-1,3-butadienes with 3-(cyano)benzopyrylium triflates and subsequent domino 'retro-Michaelitrile-addition/heterocyclization' reaction

Rashid MA; Rasool N; Appel B; Adeel M; Karapetyan V; Mkrtchyan S; Reinke H; Fischer C; Langer P

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Synthesis of 1-azaxanthones by condensation of 1,3-bis(trimethylsilyloxy)-1,3-butadienes with 3-(cyano)benzopyrylium triflates and subsequent domino 'retro-Michaelitrile-addition/heterocyclization' reaction

机译：通过1,3-双（三甲基甲硅烷氧基）-1,3-丁二烯与3-（氰基）苯并吡啶三氟甲磺酸酯的缩合反应和随后的多米诺骨牌反应（``迈克尔-还原/腈加成/杂环化''反应）合成1-氮杂蒽酮

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Functionalized 1-azaxanthones (5-oxo-5H-[1]-benzopyrano[2,3-b]pyridines) were prepared by TMSOTf-mediated condensation of 1,3-bis(trimethylsilyloxy)-1,3-butadienes with 3-cyanochromones and subsequent base-mediated domino 'retro-Michaelitrile-addition/heterocyclization' reaction. (C) 2008 Elsevier Ltd. All rights reserved.

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《Tetrahedron》 |2008年第22期|共10页
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Rashid MA; Rasool N; Appel B; Adeel M; Karapetyan V; Mkrtchyan S; Reinke H; Fischer C; Langer P;
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1; 3-BIS-SILYL ENOL ETHERS; EFFICIENT SYNTHESIS; DERIVATIVES; CHEMISTRY;

机译：1;3-双-BIS-硅醇基醚;高效合成;衍生物;化学性质;

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1. Synthesis of 1-azaxanthones by condensation of 1,3-bis(trimethylsilyloxy)-1,3-butadienes with 3-(cyano)benzopyrylium triflates and subsequent domino 'retro-Michaelitrile-addition/heterocyclization' reaction [J] . Rashid MA, Rasool N, Appel B, Tetrahedron . 2008,第22期

机译：通过1,3-双（三甲基甲硅烷氧基）-1,3-丁二烯与3-（氰基）苯并吡啶三氟甲磺酸酯的缩合反应和随后的多米诺骨牌反应（``迈克尔-还原/腈加成/杂环化''反应）合成1-氮杂蒽酮
2. Domino [3+3] annulation/ring-cleavage reactions of 1,3- bis(trimethylsilyloxy)-1,3-butadienes with 5-aryl- and 5-vinyl-3-acyl-4,5- dihydrofurans: Efficient synthesis of 5-(4-chlorobut-2-en-1-yl)- and 5-(2-aryl-2-chloroethyl)salicylates [J] . Lau M., Sher M., Villinger A., European journal of organic chemistry . 2010,第19期

机译：1,3-双（三甲基甲硅烷氧基）-1,3-丁二烯与5-芳基-和5-乙烯基-3-酰基-4,5-二氢呋喃的多米诺[3 + 3]环化/环裂解反应：高效合成5-（4-氯丁-2-烯-1-基）-和5-（2-芳基-2-氯乙基）水杨酸酯
3. Synthesis of 9-aryl-9,10-dihydrophenanthrenes by domino [3+3] annulation/ring-opening/Friedel-Crafts alkylation reactions of 1,3-bis(trimethylsilyloxy)-1,3-butadienes with 3-aroyl-5-aryl-4,5-dihydrofurans [J] . Lau M., Sher M., Villinger A., European journal of organic chemistry . 2010,第26期

机译：多米诺[3 + 3]环合/开环/ Friedel-Crafts烷基化1,3-双（三甲基甲硅烷氧基）-1,3-丁二烯与3-芳基-5的合成9-芳基-9,10-二氢菲-芳基-4,5-二氢呋喃
4. Bimetallomesogens: synthesis and mesomorphic properties of coppercomplexes of 3,3-(2-hydroxypropane-1,3-diyl)bis(azan-1yl-l-ylidene)bis(2-(4-alkoxyphenyl)prop-1-en-1-ol) [C] . Chun-Jung Chen, Chung K. Lai 2009 International Symposium on Liquid Crystal Science and Technology(2009国际液晶科技研讨会） . 2009

机译：双金属成孔剂：3,3-（2-羟基丙烷-1,3-二基）双（Azan-1yl-1-亚烷基）双（2-（4-烷氧基苯基）prop-1-en-1的铜配合物的合成和介晶性质-ol）
5. I. Synthesis of substituted naphthalenes utilizing active nickel. II. Synthesis of substituted naphthoquinones and formation of a charge transfer complex. III. Synthesis of substituted 1,4-diphenyl-2-butenes from (eta(6):eta(6)-1,4-diphenyl-1,3-butadiene)-bis(tricarbonylchromium) [D] . Forkner, Matthew W. 1988

机译：I.利用活性镍合成取代的萘。二。取代萘醌的合成和电荷转移配合物的形成。三，由（eta（6）：eta（6）-1,4-二苯基-1,3-丁二烯）-双（三羰基铬）合成取代的1,4-二苯基-2-丁烯
6. Hetero-Diels–Alder reaction of 13-bis(trimethylsilyloxy)-13-butadienes with arylsulfonylcyanides. Synthesis and antimicrobial activity of 4-hydroxy-2-(arylsulfonyl)pyridines [O] . Ibrar Hussain, Mirza Arfan Yawer, Michael Lalk, -1

机译：13-双（三甲基甲硅烷氧基）-13-丁二烯与芳基磺酰基氰化物的杂狄尔斯-阿尔德反应。 4-羟基-2-（芳基磺酰基）吡啶的合成及抑菌活性
7. Characterization studies of 1-(4-cyano-2-oxo-1,2-dihydro-1-pyridyl)-3-(4-cyano-1,2-dihydro-1-pyridyl)propane formed from the reaction of hydroxide Ion with 1,3-Bis-(4-cyano pyridinium)propane [O] . FIORI, Simone, SCHUQUEL, Ivânia T. A, SILVA, Idélcio N. da, 2011

机译：氢氧化物离子反应生成的1-（4-氰基-2-氧代-1,2-二氢-1-吡啶基）-3-（4-氰基1,2-二氢-1-吡啶基）丙烷的表征研究与1,3-双-（4-氰基吡啶鎓）丙烷
8. 1,1,3,3-Tetramethyl-2,2,4,4-Tetrakis(Trimethylsilyl)-1,3- Disilacyclobutane and Its 1,3-Digerma and 1,3-Distanna Analogs: Unexpected Products from the Reaction of Bis-(Trimethylsilyl)Bromomethyllithium with Dimethyldihalo Derivatives of Silicon, Germanium and Tin. [R] . Seyferth, D., Lefferts, J. L. 1976

机译：1,1,3,3-四甲基-2,2,4,4-四（三甲基甲硅烷基）-1,3-二硅杂环丁烷及其1,3-Digerma和1,3-Distanna类似物：来自Bis反应的意外产物 - （三甲基甲硅烷基）溴甲基锂与硅，锗和锡的二甲基二卤代衍生物。

Synthesis of 1-azaxanthones by condensation of 1,3-bis(trimethylsilyloxy)-1,3-butadienes with 3-(cyano)benzopyrylium triflates and subsequent domino 'retro-Michaelitrile-addition/heterocyclization' reaction

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