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Fatigue performance of adhesively cemented glass-, hybrid- and resin-ceramic materials for CAD/CAM monolithic restorations

机译:用于CAD / CAM整体修复的胶粘玻璃,混合和树脂陶瓷材料的疲劳性能

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Objective. To evaluate the fatigue failure load, number of cycles until failure, and survival probability of adhesively cemented materials with different microstructures (glass-, hybrid and resin-ceramic) used to manufacture CAD/CAM monolithic restorations.Methods. Disc-shaped specimens (n =15; empty set =10 mm; thickness =1.0 mm) were produced from CAD/CAM blocks as follows: feldspathic (FEL); leucite (LEU); lithium disilicate (LD); zirconia-reinforced lithium silicate (ZRLS); polymer-infiltrated ceramic network (PICN); and resin nanoceramic (RNC). Adhesive cementation was performed onto epoxy discs (dentin analogue- empty set= 10 mm; thickness = 2.5 mm). The cemented assemblies were subjected to fatigue testing using a step-stress approach (400 N-2200 N; step-size of 200 N; 10,000 cycles per step; 1.4 Hz). Fatigue data were analyzed using Kaplan-Meier and Mantel-Cox (log-rank) tests (p 0.05) and Weibull statistical analysis. Fractographic analysis was also performed.Results. All RNC specimens survived the fatigue test (100% probability of survival at 2200 N; 100,000 cycles) and presented occlusal deformation in response to loading, while all other tested materials failed in distinct loading steps with radial cracks starting from the bonding surface. LD (1146.7 N; 47,333) and ZRLS (1013.3 N; 40,666) materials obtained the highest fatigue failure loads and cycles until failure, meanwhile all PICN specimens failed during the first step (0% probability of survival at 400 N; 10,000). FEL had similar Weibull modulus to LD and ZRLS and higher than LEU for both load and number of cycles outcomes.Significance. The microstructure of adhesively cemented glass-, hybrid- and resin-ceramic CAD/CAM restorative materials influence their response during fatigue testing, which aids in suggesting the best clinical indications. (C) 2019 The Academy of Dental Materials. Published by Elsevier Inc. All rights reserved.
机译:目的。为了评估用于制造CAD / CAM整体修复体的具有不同微观结构(玻璃,混合和树脂陶瓷)的胶粘材料的疲劳破坏载荷,直到破坏的循环次数以及存活概率。圆盘形标本(n = 15;空置= 10 mm;厚度= 1.0 mm)由CAD / CAM块制成,如下所示:白榴石(LEU);二硅酸锂(LD);氧化锆增强硅酸锂(ZRLS);聚合物渗透陶瓷网络(PICN);和树脂纳米陶瓷(RNC)。在环氧树脂盘上进行粘合胶凝(牙本质类似物-空置= 10mm;厚度= 2.5mm)。使用步进应力方法(400 N-2200 N; 200 N的步长;每步10,000个循环; 1.4 Hz)对接合的组件进行疲劳测试。使用Kaplan-Meier和Mantel-Cox(对数秩)检验(p <0.05)和Weibull统计分析来分析疲劳数据。还进行了分形分析。所有RNC标本都通过了疲劳测试(在2200 N; 100000次循环下100%的存活概率),并且响应于载荷而出现咬合变形,而所有其他测试材料在明显的载荷步骤中均破裂,并从粘结表面开始出现径向裂纹。 LD(1146.7 N; 47,333)和ZRLS(1013.3 N; 40,666)材料获得了最高的疲劳失效载荷和疲劳失效周期,直到失效为止,同时所有PICN试样在第一步中均失效(在400 N下存活率为0%; 10,000)。 FEL具有与LD和ZRLS相似的Weibull模量,并且在负荷和循环次数方面均高于LEU。胶粘玻璃,混合陶瓷和树脂陶瓷CAD / CAM修复材料的微观结构会影响其在疲劳测试过程中的响应,这有助于建议最佳的临床适应症。 (C)2019牙科材料学院。由Elsevier Inc.出版。保留所有权利。

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