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Fatigue performance of adhesively cemented glass-, hybrid- and resin-ceramic materials for CAD/CAM monolithic restorations

机译:用于CAD / CAM单片修复物的粘性胶合玻璃,杂交和树脂陶瓷材料的疲劳性能

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Objective. To evaluate the fatigue failure load, number of cycles until failure, and survival probability of adhesively cemented materials with different microstructures (glass-, hybrid and resin-ceramic) used to manufacture CAD/CAM monolithic restorations.Methods. Disc-shaped specimens (n =15; empty set =10 mm; thickness =1.0 mm) were produced from CAD/CAM blocks as follows: feldspathic (FEL); leucite (LEU); lithium disilicate (LD); zirconia-reinforced lithium silicate (ZRLS); polymer-infiltrated ceramic network (PICN); and resin nanoceramic (RNC). Adhesive cementation was performed onto epoxy discs (dentin analogue- empty set= 10 mm; thickness = 2.5 mm). The cemented assemblies were subjected to fatigue testing using a step-stress approach (400 N-2200 N; step-size of 200 N; 10,000 cycles per step; 1.4 Hz). Fatigue data were analyzed using Kaplan-Meier and Mantel-Cox (log-rank) tests (p 0.05) and Weibull statistical analysis. Fractographic analysis was also performed.Results. All RNC specimens survived the fatigue test (100% probability of survival at 2200 N; 100,000 cycles) and presented occlusal deformation in response to loading, while all other tested materials failed in distinct loading steps with radial cracks starting from the bonding surface. LD (1146.7 N; 47,333) and ZRLS (1013.3 N; 40,666) materials obtained the highest fatigue failure loads and cycles until failure, meanwhile all PICN specimens failed during the first step (0% probability of survival at 400 N; 10,000). FEL had similar Weibull modulus to LD and ZRLS and higher than LEU for both load and number of cycles outcomes.Significance. The microstructure of adhesively cemented glass-, hybrid- and resin-ceramic CAD/CAM restorative materials influence their response during fatigue testing, which aids in suggesting the best clinical indications. (C) 2019 The Academy of Dental Materials. Published by Elsevier Inc. All rights reserved.
机译:客观的。为了评估疲劳破坏载荷,循环次数,直到破坏,粘合粘合材料的存活概率,具有用于制造CAD / CAM单片修复剂的不同微结构(玻璃,杂交和树脂陶瓷)。方法。如下:Feldspathic(Fel)生产圆盘形样品(N = 15;空设置= 10 mm;厚度= 1.0 mm); leucite(leu);锂末端(LD);氧化锆增强锂硅酸锂(Zrls);聚合物渗透陶瓷网络(PICN);和树脂纳米委员会(RNC)。粘合剂胶结在环氧圆盘上进行(牙本质组合物 - 空设定= 10mm;厚度= 2.5mm)。使用阶梯应力方法(400n-2200n;梯度大小为200n;每步的10,000个循环; 1.4 Hz)进行抵抗力试验。使用Kaplan-Meier和Mantel-Cox(Log-Rank)测试进行分析疲劳数据(P <0.05)和Weibull统计分析。还执行了Fretography分析。结果。所有RNC标本均存活疲劳试验(在2200N n的100%存活概率下;响应于载荷而呈现咬合变形,而所有其他测试材料在不同的加载步骤中失效,其中从粘合表面开始径向裂缝。 LD(1146.7 n; 47,333)和Zrls(1013.3 n; 40,666)材料获得了最高疲劳失效载荷和循环直到失效,同时所有PICN样本在第一步(400n N n为0%的0%的存活率)失败。 FEL与LD和Zrls类似的Weibull模量,高于Leu,用于负载和循环结果。重要性。粘合胶水玻璃 - ,杂交和树脂 - 陶瓷CAD / CAM恢复材料的微观结构影响其在疲劳试验期间的反应,这有助于提示最好的临床适应症。 (c)2019年牙科材料学院。由elsevier Inc.出版的所有权利保留。

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