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Research on Determination of Acrylamide in Fried Food by Flow Injection Chemiluminescence

机译:流动注射化学发光测定油炸食品中丙烯酰胺的研究

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In order to establish a novel flow injection chemiluminescence method for the analysis of trace acrylamide in fried foods, the acrylamide in the sample was extracted, and its effect on Luminol-Hydrogen Peroxide Chemical luminescence system to enhance the role of the determination of the conditions of the system to optimize and discuss the system. The results showed that the linear range of acrylamide was 1.0 × 10~(-6) ~ 1.0 × 10~(-3) mol/L, the correlation coefficient r = 0.9993, the detection limit was 3.95 × 10~(-8) mol/L, The relative standard deviation (RSD) of the sample was 1.3% ~ 107%, and the relative standard deviation (RSD) was 1.3% (n = 9). The method is simple and quick, low cost, practical, for the determination of fried foods in the acrylamide, the results are satisfactory.
机译:为了建立一种新的流动注射化学发光方法,用于分析油炸食品中痕量丙烯酰胺,提取样品中的丙烯酰胺,其对鲁米醇 - 过氧化氢化学发光体系的影响,提高了测定条件的作用系统优化和讨论系统。结果表明,丙烯酰胺的线性范围为1.0×10〜(-6)〜1.0×10〜(-3)mol / L,相关系数r = 0.9993,检测限为3.95×10〜(-8) MOL / L,样品的相对标准偏差(RSD)为1.3%〜107%,相对标准偏差(RSD)为1.3%(n = 9)。该方法简单快捷,成本低,实用,用于测定丙烯酰胺中的油炸食品,结果令人满意。

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