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Tensile Ductility of Liquid-Phase Sintered β-Silicon Carbide at Elevated Temperature

机译:升高温度下液相烧结β-碳化硅的拉伸延展性

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Nano-grain sized β-SiC was prepared with various additives by hot-pressing in Ar. The relative bulk densities were more than 95 %. As-sintered bodies were composed of equiaxed grains. Amorphous phase existed at grain boundaries in each as-sintered material. Tension tests were performed at the initial strain rates from 3 × 10~(-4) s~(-1) to 3 × 10~(-5) s~(-1) at 1973 - 2048 K. Tensile elongation more than 60 % was obtained. In deformed specimens, grain growth was observed. However, anisotropy of grain growth was not observed. The grain-boundary phase was vaporized during tension tests. The β phase of SiC was stable even after tension test. Therefore, critical deformation mechanism was thought to be grain-boundary sliding. Deformation behavior was influenced by the grain-boundary phase.
机译:通过在AR中热压用各种添加剂制备纳米粒大小β-SiC。相对散装密度超过95%。烧结体由等轴的晶粒组成。在每个烧结材料中存在于晶界的非晶相。在1973 - 2048K的初始应变速率下以3×10〜(-4)〜(-1)至3×10〜(-5)〜(-1)的初始应变速率进行张力试验。拉伸伸长率超过60获得%。在变形的标本中,观察到晶粒生长。然而,未观察到晶粒生长的各向异性。在张力试验期间蒸发晶粒边界相。即使在张力试验后,SiC的β相也稳定。因此,认为临界变形机制被认为是晶界滑动。变形行为受晶界阶段的影响。

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