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Microwave synthesized CuO nanoleaves as nonenzymatic glucose sensor

机译:微波合成CuO纳米叶作为非酶葡萄糖传感器

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CuO nanoleaves have been synthesized by cetyl trimethyl ammonium bromide (CTAB) assisted microwave method and characterized by powder X-ray and selected area electron diffractions, scanning and transmission electron microscopies and energy dispersive X-ray and electrochemical impedance spectroscopies. The CuO nanoleaves on graphite nonenzymatically sense glucose electrochemically. Cyclic voltammetic and chronoamperometric studies reveal the excellent catalytic activity of the modified electrode towards direct glucose oxidation. A wider linear range of glucose concentration and a shorter response time are observed. The detection limit of glucose is as low as 4μM and the CuO nanoleaves can be used as efficient electrochemical sensor.
机译:通过十六烷基三甲基溴化铵(CTAB)辅助微波法合成了CuO纳米叶,并通过粉末X射线和选择区域电子衍射,扫描和透射电子显微镜以及能量色散X射线和电化学阻抗谱进行了表征。石墨上的CuO纳米叶非酶电化学方式感测葡萄糖。循环伏安法和计时电流法研究表明,修饰电极对直接葡萄糖氧化具有出色的催化活性。观察到较宽的线性范围的葡萄糖浓度和较短的响应时间。葡萄糖的检出限低至4μM,CuO纳米叶可用作有效的电化学传感器。

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