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Process for the electrochemical oxidation of arylketones

机译:芳基酮的电化学氧化方法

摘要

The present invention provides a process for preparing arylglyoxals which comprise the steps of (a) electrochemically oxidizing an arylketone at a pH of less than about seven and at a temperature of from about -20. degree. C. to about 120° C. in the presence of an electrolyte for a sufficient period of time to form an arylacetal, and (b) subjecting said acetal to hydrolysis for a sufficient period of time and under suitable temperature and pressure conditions to form said arylglyoxal.
机译:本发明提供了制备芳基乙二醛的方法,该方法包括以下步骤:(a)在小于约7的pH值和约-20的温度下电化学氧化芳基酮。度。在电解质的存在下,在约200℃至约120℃的温度下持续足够的时间以形成芳基缩醛,以及(b)在适当的温度和压力条件下使所述缩醛水解足够的时间以形成所述芳基缩醛。芳基乙二醛。

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