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METHOD FOR CARRYING OUT MULTIPHASE ALDOL CONDENSATION REACTIONS TO OBTAIN MIXED α,β-UNSATURATED ALDEHYDES

机译:进行多相ALDOL缩合反应制得混和的α,β-不饱和醛的方法

摘要

The invention relates to a continuous method for carrying out a multiphase aldol condensation reaction to obtain mixed α,β-unsaturated aldehydes by reacting a mixture of two aliphatic aldehydes having different numbers of carbon atoms, i.e. 2 to 5, in the molecule in a vertical tubular reactor in a concurrent flow in the presence of an aqueous solution of a basically reacting compound. In said method, the aldehyde mixture is dispersed in the aqueous phase in the form of drops, and the aqueous solution of the basically reacting compound flows through the tubular reactor as a continuous phase in laminar conditions.
机译:本发明涉及一种连续方法,该方法通过使两个具有不同碳原子数,即2至5的脂族醛的混合物在垂直方向上的分子中反应,进行多相醇醛缩合反应以获得混合的α,β-不饱和醛管状反应器在基本反应的化合物的水溶液存在下并发流动。在所述方法中,醛混合物以液滴形式分散在水相中,并且基本反应的化合物的水溶液在层流条件下作为连续相流过管式反应器。

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