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METHOD FOR RAPID DETECTION organic and inorganic perchlorate

机译:快速检测有机和无机高氯酸盐的方法

摘要

1. A method for detecting explosives based on inorganic and organic perchlorates, comprising a contact surface with the sampling at the suspicious object explosives content of the soft porous material, bringing a selected sample into contact with a cationic dye in a polar solvent, separation of the resulting solution on the sorption layer of a stationary phase the identification of the presence of the perchlorate ion visual control offset colored zone of its ion associate behind the front rastvoritelya.2. A method according to claim 1, characterized in that the sorption layer of the stationary phase may be used at least one of the adsorbents: silica, alumina, tsellyuloza.3. A method according to claim 1, characterized in that the cationic dye is used as a diamond zelenyy.4. A method according to claim 1, characterized in that the polar solvent can be used acetone, tetrahydrofuran, acetonitrile, mixtures thereof or mixtures thereof with vodoy.5. A method according to claim 1, characterized in that, in order to improve imaging contrast analysis, the cationic dye is additionally added a non-ionic dye of a different color to indicate the solvent front boundary or outer loop, which color change characterized by the presence perchlorate.
机译:1.一种用于检测基于无机和有机高氯酸盐的炸药的方法,该方法包括在软质多孔材料的可疑物品的爆炸物含量处取样的接触面,使选定的样品与极性溶剂中的阳离子染料接触,分离出所得溶液在固定相吸附层上的识别,确定存在于前拉丝沸石后方的高氯酸根离子视觉控制偏色区域的存在。2。 2.根据权利要求1所述的方法,其特征在于,所述固定相的吸附层可以使用至少一种吸附剂:二氧化硅,氧化铝,tsellyuloza.3。 2.根据权利要求1所述的方法,其特征在于,所述阳离子染料被用作钻石zelenyyy。4。 2,根据权利要求1的方法,其特征在于极性溶剂可以使用丙酮,四氢呋喃,乙腈,它们的混合物或它们与伏都的混合物。5。 2.根据权利要求1所述的方法,其特征在于,为了改善成像对比度分析,另外向阳离子染料添加不同颜色的非离子染料以指示溶剂的前边界或外环,该颜色变化的特征在于存在高氯酸盐。

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