首页> 外国专利> Extraction Procedure of unsaponifiable fraction contained in oil or Shortening from microorganism comprising stage of transformation of such Oils, alcoholic solvent extraction with at least 5 Carbon Atoms or one or two Oxygen Atoms INSAP fraction; Onificable; and use of HMDS.

Extraction Procedure of unsaponifiable fraction contained in oil or Shortening from microorganism comprising stage of transformation of such Oils, alcoholic solvent extraction with at least 5 Carbon Atoms or one or two Oxygen Atoms INSAP fraction; Onificable; and use of HMDS.

机译:油中所含不皂化物馏分或从微生物中缩短的提取程序,包括此类油的转化阶段,用至少5个碳原子或一或两个氧原子INSAP馏分进行的醇溶剂提取;有意义的和HMDS的使用。

摘要

The present invention relates to an extraction process of an unsaponifiable fraction contained in an oil or a vegetable butter, in an oil originating from a micro-organism, in a concentrate of oil or butter or of oil originating from a micro-organism, or in a co-product of the refining industry for vegetable oils, such as deodorisation exhaust and distillates of physical refining, or oils originating from micro-organisms, comprising at least: A) a transformation step of said oils, of said butter or said co-product of the refining industry for vegetable oils or oils originating from micro-organisms in hydro-alcoholic solution, especially via a saponification step, and B) an extraction step of the hydro-alcoholic solution in which the fatty fraction is separated from unsaponifiable fraction by liquid/liquid extraction, said process being characterised in that at least the liquid/liquid extraction step of the step B is performed by using a first solvent system comprising a solvent content selected from the solvents comprising at least 5 carbon atoms and one or two oxygen atoms in the form of either ether function, or ketone function, or ester function, of at least 50% in volume relative to the total volume of the first solvent system, as well as fractions obtained by said process.
机译:本发明涉及油或植物黄油,微生物来源的油,油或黄油或微生物来源的油的浓缩物中或油中的不皂化物馏分的提取方法。植物油精制工业的副产品,例如脱臭废气和物理精制馏出物,或源自微生物的油,至少包括:A)所述油,所述黄油或所述共聚油的转化步骤植物油精制工业的产品或水醇溶液中微生物产生的油,特别是通过皂化步骤,以及B)水醇溶液的提取步骤,其中脂肪馏分通过不皂化馏分与不皂化馏分分离液/液萃取,所述方法的特征在于至少步骤B的液/液萃取步骤通过使用包含溶剂含量的第一溶剂体系进行选自包含至少5个碳原子和一个或两个氧原子的溶剂,该溶剂的形式为相对于第一溶剂体系的总体积至少50%体积的醚官能或酮官能或酯官能,以及通过所述方法获得的馏分。

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