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An improved experimental procedure of separating a composite thermoluminescence glow curve into its components

机译:将复合热致发光辉光曲线分离为其分量的改进实验程序

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摘要

We present an improved experimental procedure of separating a composite thermoluminescence glow curve into its components. Careful monitoring of the isothermal cleaning process using the initial rise method ensures the complete thermal removal of TL peaks. Digital subtraction of two experimental TL glow curves yields individual experimental TL glow peaks. Several standard methods (initial rise and whole glow curve) are used to obtain the energy values and frequency factors of the traps. The method has been used successfully to analyze the well-known composite TL glow curve of the dosimetric material LiF (TLD-100). The limitations of the method are illustrated by analyzing the highly complex TL glow curve of a UV irradiated synthetic calcite consisting of at least 6 TL peaks. Although the method works best for TL glow curves described by first order kinetics, it should also be applicable to more general kinetics. (C) 2000 Elsevier Science Ltd. All rights reserved. [References: 8]
机译:我们提出了一种改进的实验程序,将复合热致发光辉光曲线分离为其组成部分。使用初始上升方法仔细监控等温清洗过程,可确保完全去除TL峰的热量。对两个实验TL辉光曲线进行数字减法会产生单个实验TL辉光峰。几种标准方法(初始上升和整个辉光曲线)用于获取陷阱的能量值和频率因子。该方法已成功用于分析剂量材料LiF(TLD-100)的众所周知的复合TL辉光曲线。通过分析由至少6个TL峰组成的UV辐射合成方解石的高度复杂的TL辉光曲线,可以说明该方法的局限性。尽管该方法最适合一阶动力学描述的TL辉光曲线,但它也应适用于更一般的动力学。 (C)2000 Elsevier ScienceLtd。保留所有权利。 [参考:8]

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