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The fabrication of highly ordered and visible-light-responsive Fe-C-N-Codoped TiO2 nanotubes

机译:高序和可见光响应的Fe-C-N-掺杂的TiO2纳米管的制备

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摘要

A one-step method for the fabrication of Fe-C-N-codoped TiO2 nanotubes by electrochemical anodization is reported. The proposed method is both simple and efficient. The prepared samples were annealed at 550 degrees C for 3 h. The resulting nanotubes were characterized by SEM, XRD, XPS, EDX and UV-vis spectrophotometer. The results showed that the average tube diameter of the nanotubes was 70 nm and wall thickness was 20 nm and the average tube length was 2.4 mu m. The doped TiO2 nanotubes exhibited strong absorption in the visible-light region. The maximum photocurrent efficiency measured under solar simulator was 2.7%.
机译:报道了一种通过电化学阳极氧化制备Fe-C-N掺杂的TiO2纳米管的一步法。所提出的方法既简单又有效。制备的样品在550摄氏度下退火3小时。所得的纳米管通过SEM,XRD,XPS,EDX和UV-vis分光光度计进行表征。结果表明,纳米管的平均管径为70nm,壁厚为20nm,平均管长为2.4μm。掺杂的TiO2纳米管在可见光区域表现出强吸收性。在太阳模拟器下测得的最大光电流效率为2.7%。

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