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The Influence of Calcination Temperature on Phase and Morphology of Ba(Sn_(0.05)Ti_(0.95))O_3 Powders Synthesized via Solid State Reaction Method and Combustion Technique

机译:煅烧温度对固相反应法和燃烧技术合成Ba(Sn_(0.05)Ti_(0.95))O_3粉末相和形貌的影响

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摘要

Barium stannate titanate [Ba(Sn_(0.05)Ti_(0.95))O_3;;BST5] powders were synthesized via a solid state reaction and combustion techniques. The single perovskite phase of BST5 powders was found with calcinations temperature of 1200 deg C for both techniques. The percent of perovskite and lattice parameter a increased with an increase of calcinations temperature. The average particle size increased from 0.54 to 0.86 mu m for the solid state reaction method and 0.35 to 0.78 mu m for the combustion technique when increasing calcinations temperature from 600 to 1200 deg C. The average particle size from the combustion technique was smaller than the solid state reaction method.
机译:通过固相反应和燃烧技术合成了钛酸钡钛酸盐[Ba(Sn_(0.05)Ti_(0.95))O_3 ;; BST5]粉末。对于这两种技术,均发现BST5粉末的钙钛矿相的煅烧温度为1200℃。钙钛矿和晶格参数α的百分比随煅烧温度的升高而增加。当将煅烧温度从600℃提高到1200摄氏度时,固态反应方法的平均粒径从0.54增至0.86微米,燃烧技术的平均粒径从0.35增至0.78微米。燃烧技术的平均粒径小于固态反应法。

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