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Made in Switzerland: 25 Years of Swiss Ion Chromatography

机译:瑞士制造:25年的瑞士离子色谱法

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摘要

Metrohm is a well-established company in the field of ion analysis. Back in 1948, it manufactured the first pH meter. Not quite so long ago, the company also moved into ion chromatography. The achievements in its services to users are all the more important: any user can perform ion chromatographic analyses successfully! Following the successful launch of an electrochemical HPLC detector in 1981, a conductivity detector was developed in 1983. Very soon the development team realized that this task was achievable, but to obtain a stable baseline and low detection limits, the entire analytical system had to be optimized - from the high-pressure pump through capillaries to the separation column. In 1987, Metrohm presented its first ion chromatograph, the "690 Ion Chromatograph". This instrument combined an injector (manual sample injection), separation column, detector, and control electronics in a single housing and relied on single-column ion chromatography with electronic suppression. It proved that ion chromatography (IC) can be successful even without chemical suppression. For better or worse, a decision had to be made in favor of electronic suppression, because chemical suppression was at that time protected by patents and therefore not available. Although originally a hurdle, this might be precisely the reason why the conductivity detector is still the best on the market.
机译:瑞士万通在离子分析领域是一家实力雄厚的公司。早在1948年,它就制造了第一台pH计。不久之前,该公司还涉足离子色谱法。在为用户提供服务方面取得的成就更为重要:任何用户都可以成功进行离子色谱分析!在1981年成功推出电化学HPLC检测器之后,1983年开发了电导率检测器。开发团队很快意识到这一任务是可以实现的,但是要获得稳定的基线和低检测限,必须对整个分析系统进行优化。优化-从高压泵到毛细管再到分离柱。 1987年,瑞士万通推出了第一台离子色谱仪,即“ 690离子色谱仪”。该仪器将进样器(手动进样),分离柱,检测器和控制电子设备组合在一个外壳中,并依靠具有电子抑制功能的单柱离子色谱法。事实证明,即使不进行化学抑制,离子色谱(IC)也可以成功。不管好坏,都必须做出支持电子抑制的决定,因为化学抑制当时受到专利保护,因此无法获得。尽管最初是一个障碍,但这可能正是电导率检测器仍然是市场上最好的检测器的原因。

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