An Expeditious Assembly of 3,4-Benzannulated 8-Oxabicyclo[3.2.1]octane Systems by [2+2+2] Alkyne Cyclotrimerisation: Total Synthesis of (-)-Bruguierol A

Chepuri V. Ramana; Sumanth R. Salian; Rajesh G. Gonnade

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An Expeditious Assembly of 3,4-Benzannulated 8-Oxabicyclo[3.2.1]octane Systems by [2+2+2] Alkyne Cyclotrimerisation: Total Synthesis of (-)-Bruguierol A

机译：[2 + 2 + 2]炔烃环三聚反应可快速组装3,4-苯甲基化的8-氧杂双环[3.2.1]辛烷体系：（-）-Bruguierol A的全合成

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摘要

Facile construction of benzene-fused 8-oxabicyclo[3.2.1]oc-tane systems by employing a cross alkyne cyclotrimerisation reaction was explored. With this procedure, (-)-bruguierol A was synthesised, and its absolute configuration was established.

机译：探索了通过使用交叉炔烃环三聚反应的结构轻松的苯稠合的8-氧杂双环[3.2.1] oc-tane系统的构建。用这种方法，合成了（-）-bruguierol A，并确定了它的绝对构型。

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《European journal of organic chemistry》 |2007年第33期|共4页
作者
Chepuri V. Ramana; Sumanth R. Salian; Rajesh G. Gonnade;
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正文语种 eng
中图分类有机化学;
关键词
Total synthesis; Epoxidation; Cyclotrimerisation; Wilkinson's catalyst;

机译：全合成;环氧化;环三聚;威尔金森催化剂;

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1. An Expeditious Assembly of 3,4-Benzannulated 8-Oxabicyclo[3.2.1]octane Systems by [2+2+2] Alkyne Cyclotrimerisation: Total Synthesis of (-)-Bruguierol A [J] . Chepuri V. Ramana, Sumanth R. Salian, Rajesh G. Gonnade European journal of organic chemistry . 2007,第33期

机译：[2 + 2 + 2]炔烃环三聚反应可快速组装3,4-苯甲基化的8-氧杂双环[3.2.1]辛烷体系：（-）-Bruguierol A的全合成
2. First examples of Friedel-Crafts alkylation using ketals as alkylating agents: an expeditious access to the benzene-fused 8-oxabicyclo[3.2.1]octane ring system [J] . Jun-Fa Fan, Yikang Wu, Yu-Lin Wu Journal of the Chemical Society, Perkin Transactions 1 . 1999,第9期

机译：使用缩酮作为烷基化剂的Friedel-Crafts烷基化的第一个例子：迅速进入苯稠合的8-氧杂双环[3.2.1]辛烷环系统
3. Stereoselective Synthesis of 8-Oxabicyclo[3.2.1]octane-2,3,4,6,7-pentols and Total Asymmetric Synthesis of 2,6-Anhydrohepturonic Acid Derivatives and of #beta#-C-manno-Pyranosides Suitable for the Construction of (1->3)-C,C-Linked Trisaccharides [J] . Patrick Gerber, Pierre Vogel Helvetica chimica acta . 2001,第6期

机译：立体选择性合成8-氧杂双环[3.2.1]辛烷-2,3,4,6,7-戊醇和完全不对称合成2,6-脱水庚二酸衍生物和＃β＃-C-甘露聚糖-吡喃糖苷（1-> 3）-C，C联三糖的构建
4. The cobalt-mediated [2+2+2] cycloaddition of alkynes to heterocycles: I. The total synthesis of (+/-)-strychnine II. The activation of pyridones, oxazoles, and thiazoles. [D] . Eichberg, Michael Joseph. 2001

机译：炔烃与杂环的钴介导的[2 + 2 + 2]环加成反应：I.（+/-）-士翠宁的总合成II。吡啶酮，恶唑和噻唑的活化。
5. Synthesis of Highly Functionalised Enantiopure Bicyclo3.2.1- octane Systems from Carvone [O] . Antonio Abad, Consuelo Agulló, Ana C. Cuñat, 2004

机译：由香芹酮合成高功能对映纯双环3.2.1-辛烷体系
6. An Expeditious Assembly of 3,4-Benzannulated-8-oxabicyclo3:2:1octane Systems [O] . O. Venkata Subba Raju, Y.V. Rami Reddy 2013

机译：3,4- Benzannulated-8-oxabicyclo 3：2：1辛烷系统的迅速组装

An Expeditious Assembly of 3,4-Benzannulated 8-Oxabicyclo[3.2.1]octane Systems by [2+2+2] Alkyne Cyclotrimerisation: Total Synthesis of (-)-Bruguierol A

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