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首页> 外文期刊>Journal of separation science. >Determination of polychlorinated dibenzo‐ pp ‐dioxins and polychlorinated dibenzofurans, and dioxin‐like polychlorinated biphenyls in human serum using programmable‐temperature vaporization gas chromatography with high‐resolution mass spectrometry
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Determination of polychlorinated dibenzo‐ pp ‐dioxins and polychlorinated dibenzofurans, and dioxin‐like polychlorinated biphenyls in human serum using programmable‐temperature vaporization gas chromatography with high‐resolution mass spectrometry

机译：使用具有高分辨率质谱法的可编程 - 温度汽化气相色谱法测定人血清中多氯二苯并辛和聚氯二苯苄酯，以及高分辨率质谱法的二恶蛋白样多氯联苯

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Abstract > The determination of polychlorinated dibenzo‐ p ‐dioxins and polychlorinated dibenzofurans, and dioxin‐like polychlorinated biphenyls in blood from a non‐occupational population is essential for the investigation of adverse health effects from these pollutants. In this study, a sensitive method based on programmable‐temperature vaporization with large‐volume injection coupled with gas chromatography with high‐resolution mass spectrometry was developed to determine these pollutants in 1–2?mL of human serum samples. Various key parameters of programmable‐temperature vaporization injector, including vent temperature, vent time, vent flow, transfer temperature and transfer time were optimized by factorial design. The accuracy and precision as well as applicability were assessed by determining polychlorinated dibenzo‐ p ‐dioxins, polychlorinated dibenzofurans, and dioxin‐like polychlorinated biphenyls in calibration standard solutions, standard reference materials and real human serum samples from non‐occupational population. The method detection limits of polychlorinated dibenzo‐ p ‐dioxins and polychlorinated dibenzofurans, and dioxin‐like polychlorinated biphenyls were 1.5–9.0 and 0.005–0.02?ng/kg wet weight, respectively. By comparing with typically splitless injection, the application of programmable‐temperature vaporization injector could effectively lead to higher detectable rate of polychlorinated dibenzo‐ p ‐dioxins and polychlorinated dibenzofurans, and dioxin‐like polychlorinated biphenyls in 1–2?mL of human serum samples. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“main”> <标题类型=“main”>摘要</标题> >聚氯氯Dibenzo- p </ i> -dioxins和多氯二苯并呋喃的测定，以及二恶英样多氯联苯在非职业人口中的血液中对于对这些污染物的不良健康影响的调查至关重要。在该研究中，开发了一种基于具有大容量注射的可编程 - 温度蒸发的敏感方法，与高分辨率质谱相结合，以确定这些污染物1-2毫升人血清样品。通过因子设计优化了可编程温度汽化喷射器的各种关键参数，包括排气温度，排气时间，通气流，转移温度和转移时间。通过在校准标准溶液中测定聚氯氯二苯苄 - ，多氯二苯并氯脲和二恶英样的多氯联苯，标准参考材料和来自非-occupational人口。聚氯氯二苯苄 - -diOxins和聚氯二氯苯酚和二恶英的多氯联苯的方法检测限率分别为1.5-9.0和0.005-0.02〜Ng / kg湿重。通过与典型的不分流注射进行比较，可编程 - 温度汽化喷射器的应用可以有效地导致更高的多氯二苯并辛-1-吡喃和聚氯二苯并呋喃的可检测速率，1-2中的二恶蛋白样多氯联苯？Ml的人血清样品。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第17期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Lei&option=202" target="_blank" rel="nofollow">Zhang Lei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhong Yuxin&option=202" target="_blank" rel="nofollow">Zhong Yuxin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Xin&option=202" target="_blank" rel="nofollow">Liu Xin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bao Yan&option=202" target="_blank" rel="nofollow">Bao Yan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhao Yunfeng&option=202" target="_blank" rel="nofollow">Zhao Yunfeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Yongning&option=202" target="_blank" rel="nofollow">Wu Yongning;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cai Zongwei&option=202" target="_blank" rel="nofollow">Cai Zongwei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Jingguang&option=202" target="_blank" rel="nofollow">Li Jingguang;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>The Key Laboratory of Food Safety Risk AssessmentMinistry of Health (CFSA) and China National Center for Food Safety Risk AssessmentBeijing China;</p> <p>Department of Pancreatogastric Surgery National Cancer Center/Cancer HospitalChinese Academy of Medical Science and Peking Union Medical CollegeBeijing China;</p> <p>The Key Laboratory of Food Safety Risk AssessmentMinistry of Health (CFSA) and China National Center for Food Safety Risk AssessmentBeijing China;</p> <p>The Key Laboratory of Food Safety Risk AssessmentMinistry of Health (CFSA) and China National Center for Food Safety Risk AssessmentBeijing China;</p> <p>The Key Laboratory of Food Safety Risk AssessmentMinistry of Health (CFSA) and China National Center for Food Safety Risk AssessmentBeijing China;</p> <p>The Key Laboratory of Food Safety Risk AssessmentMinistry of Health (CFSA) and China National Center for Food Safety Risk AssessmentBeijing China;</p> <p>State Key Laboratory of Environmental and Biological AnalysisHong Kong Baptist UniversityHong Kong China;</p> <p>The Key Laboratory of Food Safety Risk AssessmentMinistry of Health (CFSA) and China National Center for Food Safety Risk AssessmentBeijing China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=dioxins&option=203" rel="nofollow">dioxins;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=human serum&option=203" rel="nofollow">human serum;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=large‐volume injection&option=203" rel="nofollow">large‐volume injection;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=programmable‐temperature vaporization&option=203" rel="nofollow">programmable‐temperature vaporization;</a> </p> <div class="translation"> 机译：二恶英;人血清;大批量注射;可编程 - 温度蒸发; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a 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飞行时间质谱法为发展中国家定量分析多氯二苯并对二恶英和多氯二苯并呋喃</span> </p> </li> <li> <div> <b>8. </b><a class="enjiyixqcontent" href="/ntis-science-report_pb_thesis/020711095158.html">Comparative Analysis of Polychlorinated Dibenzo-'p'-dioxin and Dibenzofuran Congeners in Great Lakes Fish Extracts by Gas Chromatography-Mass Spectrometry and In vitro Enzyme Induction Activities</a> <b>[R] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zacharewski, T.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zacharewski, T.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Safe, L.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Safe, L.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Safe, S.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Safe, S.,</a> <span>1989</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：大湖鱼提取物中多氯二苯并-d'-二恶英和二苯并呋喃同系物的气相色谱 - 质谱和体外酶诱导活性对比分析</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_detail_thesis/0201293261552.html">意大利的金枪鱼、箭鱼、鸬鹚以及家燕等体内的多氯萘、多氯联苯、多氯二苯—p—二恶英、多氯二苯并呋喃以及p,p′—DDE</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kurunthachalam Kannan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Kurunthachalam Kannan</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Simonetta Corsoline&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Simonetta Corsoline</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Takashi Imagaws&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Takashi Imagaws</a> <span> <a href="/journal-cn-57570/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . AMBIO－人类环境杂志 </a> </span> <span> . 2002</span><span>,第3期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-journal-chromatography_thesis/0201246927413.html">同位素稀释气相色谱-离子阱二级质谱法测定牛奶中残留的二恶英类多氯联苯</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=丁罡斗&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 丁罡斗</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李翔&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李翔</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘汉霞&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘汉霞</a> <span> <a href="/journal-cn-14390/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 色谱 </a> </span> <span> . 2008</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" 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