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Effects of micro‐nano titania contents and maleic anhydride compatibilization on the mechanical performance of polylactide

机译：微纳米二氧化钛含量和马来酸酐相容对聚丙烯酯机械性能的影响

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Abstract > The first aim of this study was to compare influences of various contents of the micro‐ (200?nm) and nano (50?nm)‐sized titania (TiO <sub>2</sub> ) particles especially on the mechanical performance of the polylactide (PLA) biopolymer. Micro‐ and nano‐composites were prepared by twin‐screw extruder melt mixing, while the specimens were shaped by compression molding. Scanning electron microscope analyses and mechanical tests revealed that due to the most efficient uniform distribution in the matrix, the best improvements in the strength, elastic modulus, and fracture toughness values could be obtained either by using 5 wt% micro‐TiO <sub>2</sub> or by only 2 wt% nano‐TiO <sub>2</sub> particles. The second purpose of this study was to investigate influences of using maleic anhydride (MA)‐grafted copolymer (PLA‐g‐MA) compatibilization on the performance of one nanocomposite composition. Due to the improved chemical interfacial adhesion, use of PLA‐g‐MA compatibilization for the specimen of PLA/2 wt% n‐TiO <sub>2</sub> composition resulted in the highest improvements in the mechanical performance of neat PLA. The improvements were 14% in tensile strength, 20% in flexural modulus, and as much as 67% in fracture toughness. Thermal behavior of all specimens was also observed by differential scanning calorimetry and thermogravimetric analyses. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 本研究的首次目的是比较微生物（200〜Nm）和纳米（50μm）的各种含量的影响（50？nm）的二氧化钛（TiO <sub> 2 </ sub> ）颗粒，尤其是聚丙环（PLA）生物聚合物的机械性能。通过双螺杆挤出机熔融混合制备微型和纳米复合材料，而试样通过压缩成型而成。扫描电子显微镜分析和机械测试显示，由于基质中最有效的均匀分布，通过使用5wt％的微型TiO可以获得强度，弹性模量和断裂韧性值的最佳改进 <sub> 2 </ sub> 或者只有2wt％nano-tio <sub> 2 </ sub> 粒子。该研究的第二个目的是研究使用马来酸酐（MA） - 移植的共聚物（PLA-G-MA）相容对一种纳米复合材料组合物的性能的影响。由于改善的化学界面粘附，使用PLA-G-MA相容为PLA / 2wt％N-TiO的样品 <sub> 2 </ sub> 组成导致纯PLA的机械性能的最高改善。抗拉强度的改善为14％，弯曲模量为20％，骨折韧性高达67％。还通过差示扫描量热法和热重分析观察所有样本的热行为。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29566/'>《Polymer Composites》</a> <b style="margin: 0 2px;">|</b><span>2020年第2期</span><b style="margin: 0 2px;">|</b><span>共14页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/7852.html" title="增强塑料、填充塑料">增强塑料、填充塑料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=maleic anhydride&option=203" rel="nofollow">maleic anhydride;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=mechanical properties&option=203" rel="nofollow">mechanical properties;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=micro titania&option=203" rel="nofollow">micro titania;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nano titania&option=203" rel="nofollow">nano titania;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polylactide&option=203" rel="nofollow">polylactide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thermal properties&option=203" rel="nofollow">thermal properties;</a> </p> <div class="translation"> 机译：马来酸酐;机械性能;微型二氧化钛;纳米二氧化钛;聚丙烯酸酯;热性能; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024545296.html">Effects of micro‐nano titania contents and maleic anhydride compatibilization on the mechanical performance of polylactide</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=&option=202" target="_blank" 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韩国专利： --> KR100816800B1 </span> <span> . 2008-03-26</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用尼龙6和酸酐马来聚丙烯作为增容剂的含纳米尺寸粘土的聚丙烯纤维的制造方法以及通过该方法制造的含纳米尺寸粘土的聚丙烯纤维 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130431997213.html">THE PROCESSING METHOD OF POLYPROPYLENE/CLAY NANOCOMPOSITE FIBER AND NANOCOMPOSITE FIBER PRODUCED THEREOF USING NYLON 6 AND ANHYDRIDE MALEIC POLYPROPYLENE AS COMPATIBILIZER</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR20070115133A </span> <span> . 2007-12-05</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：聚丙烯/粘土纳米复合纤维的制备方法及其以尼龙6和酸酐马来酸聚丙烯为相容剂制备的纳米复合纤维的制备方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130426985137.html">POLYLACTIC ACID-CONTAINING BIODEGRADABLE RESIN COMPOSITION CONTAINING A COMPOUND OF GLYCIDYL METHACRYLATE AND MALEIC ANHYDRIDE AS A COMPATIBILIZER, OR A COMPOUND OF THE MALEIC ANHYDRIDE AND OCTENYL SUCCINIC ANHYDRIDE</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR20100108683A </span> <span> . 2010-10-08</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含甲基丙烯酸缩水甘油酯和马来酸酐的化合物或相容剂，或马来酸酐和辛基环辛酯的化合物的含聚乙酸的生物可降解树脂组合物 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" 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