Carbon‐Doped Metal Oxide Nanoparticles Prepared from Metal Nitrates in Supercritical CO2‐Enabled Polymer Nanoreactors

Jiang Nina; Wang Yiwei; Li Danyang; Niu Jie; Wang Shibin; Chen Aizheng

摘要

Abstract > Various C‐doped metal oxide nanoparticles (NPs) are prepared from metal nitrates in poly‐(methyl vinyl ether‐ co ‐maleic anhydride) (PVM/MA) nanoreactors. The loading of metal nitrates in the nanoreactors is realized via a process of solution‐enhanced dispersion by supercritical CO <sub>2</sub> . When the temperature exceeds the thermal decomposition temperature of the nitrates, the nitrates‐loaded nanoreactors transform into C‐doped metal oxide NPs. ZnO, NiO, and Co <sub>3</sub> O <sub>4</sub> NPs as representative of the doped oxides are successfully fabricated. A precise control over the doping concentration and doping site in the lattice is achieved by changing the mass ratio between PVM/MA and metal nitrate. The controllable carbon doping avoids undesirable aggregation of carbon species and metal oxide NPs, endows the NPs with broad and strong absorption bands in the visible light region, and creates channels for separation of photo‐generated electrons and holes. In this regard, the resultant C‐doped metal oxide NPs exhibit excellent photocatalytic, photo‐induced antibacterial, and photothermal performances. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 各种C掺杂的金属氧化物纳米颗粒（NPS）由聚 - （甲基乙烯基醚 - 的金属硝酸盐制备 co </ i> - Maleic酸酐）（PVM / mA）纳米反应器。通过超临界CO可以通过溶液增强的分散方法实现纳米反应器中的金属硝酸盐的装载 <sub> 2 </ sub> 。当温度超过硝酸盐的热分解温度时，硝酸盐加载的纳米反应器转化成C掺杂金属氧化物NPS。 Zno，nio和co <sub> 3 </ sub> O. <sub> 4 </ sub> 作为掺杂氧化物代表的NPS成功制造。通过改变PVM / MA和金属硝酸盐之间的质量比来实现对掺杂浓度和掺杂位点的精确控制。可控碳掺杂避免了碳物质和金属氧化物NP的不希望的聚集，赋予可见光区域中具有宽且强的吸收带的NPS，并产生用于分离光产生的电子和孔的通道。在这方面，所得的C掺杂金属氧化物NPS表现出优异的光催化，光诱导的抗菌和光热性能。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-28901/'>《Particle & Particle Systems Characterization: Measurement and Description of Particle Properties and Behavior in Powders and Other Disperse Systems》</a> <b style="margin: 0 2px;">|</b><span>2019年第9期</span><b style="margin: 0 2px;">|</b><span>共11页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jiang Nina&option=202" target="_blank" rel="nofollow">Jiang Nina;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Yiwei&option=202" target="_blank" rel="nofollow">Wang Yiwei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Danyang&option=202" target="_blank" rel="nofollow">Li Danyang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Niu Jie&option=202" target="_blank" rel="nofollow">Niu Jie;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Shibin&option=202" target="_blank" rel="nofollow">Wang Shibin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Aizheng&option=202" target="_blank" rel="nofollow">Chen Aizheng;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>College of Chemical EngineeringHuaqiao UniversityXiamen 361021 P. R. China;</p> <p>College of Chemical EngineeringHuaqiao UniversityXiamen 361021 P. R. China;</p> <p>College of Chemical EngineeringHuaqiao UniversityXiamen 361021 P. R. China;</p> <p>College of Chemical EngineeringHuaqiao UniversityXiamen 361021 P. R. China;</p> <p>Fujian Provincial Key Laboratory of Biochemical Technology (Huaqiao University)Xiamen 361021 P. R. China;</p> <p>College of Chemical EngineeringHuaqiao UniversityXiamen 361021 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=controllable carbon doping&option=203" rel="nofollow">controllable carbon doping;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=metal oxide nanoparticles&option=203" rel="nofollow">metal oxide nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polymer nanoreactors&option=203" rel="nofollow">polymer nanoreactors;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=supercritical CO2&option=203" rel="nofollow">supercritical CO2;</a> </p> <div class="translation"> 机译：可控碳掺杂;金属氧化物纳米颗粒;聚合物纳米反应器;超临界CO2; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024384904.html">Carbon‐Doped Metal Oxide Nanoparticles Prepared from Metal Nitrates in Supercritical CO2‐Enabled Polymer Nanoreactors</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jiang Nina&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Jiang Nina,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Yiwei&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Wang Yiwei,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Danyang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Li Danyang,</a> <a href="/journal-foreign-28901/" target="_blank" rel="nofollow" class="tuijian_authcolor">Particle & Particle Systems Characterization: Measurement and Description of Particle Properties and Behavior in Powders and Other Disperse Systems .</a> <span>2019</span><span>,第9期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：碳掺杂金属氧化物纳米颗粒，由金属硝酸盐制备在超临界CO2的聚合物纳米反应器中</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704021717284.html">Well-defined gold nanoparticle@N-doped porous carbon prepared from metal nanoparticle@metal-organic frameworks for electrochemical sensing of hydrazine</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Juan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Yang Juan,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhao Faqiong&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zhao Faqiong,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zeng Baizhao&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zeng Baizhao </a> <a href="/journal-foreign-27299/" target="_blank" rel="nofollow" class="tuijian_authcolor">RSC Advances .</a> <span>2016</span><span>,第28期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：明确明确的金纳米粒子@ N掺杂多孔碳，由金属纳米粒子@金属 - 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