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Enhancement of absorbing frequency and photo-catalytic performance by temperature treatment of composites Fe3O4-AC nanoparticle

机译:复合材料Fe3O4-AC纳米粒子温度处理吸收频率和光催化性能的增强

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摘要

Structural and bonding characteristics of multifunction nanocomposite Fe3O4-activated carbon (Fe3O4-AC) for various annealing temperatures; 500 degrees C, 700 degrees C, and 900 degrees C have been studied by using X-ray diffraction (XRD) and Fourier transforms infrared spectroscopy (FTIR), respectively. Crystallite size and OAH bonds were decreases with increasing the annealing temperature. For electromagnetic (EM) properties from the Vector Network Analyzer (VNA) shows working frequency increases from 6 GHz to 6.8 GHz and the bandwidth widening increase up to 3.3 GHz with increasing the annealing temperature, and the reflection loss (RL) values for all composites in this study shows less than -10 dB indicated suitability for EM absorber. The photocatalytic ability was determined by using ultra violet visible (Uv-Vis) spectroscopy and methylene blue (MB) solution as a liquid waste test model. The stable annealing temperatures for absorber EM is 900 degrees C and for the photo-catalytic application is 500 degrees C. In this study shows temperature play an important role in stabilizing the performance of multifunction composite of Fe3O4-AC nanoparticle for EM absorber and for liquid waste purifying catalyst. (C) 2019 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.
机译:各种退火温度的多功能纳米复合Fe3O4 - 活性炭(Fe3O4-AC)的结构和粘合特性;通过使用X射线衍射(XRD)和傅里叶变换红外光谱(FTIR)已经研究了500℃,700℃和900℃。随着退火温度的增加,微晶尺寸和OAH键会降低。对于来自矢量网络分析器(VNA)的电磁(EM)性质,显示工作频率从6 GHz到6.8 GHz增加,随着退火温度的增加,带宽扩大增加了3.3GHz,以及所有复合材料的反射损耗(RL)值在本研究中,显示器显示少于-10dB对EM吸收器的适用性。通过使用超紫可见(UV-VIS)光谱和亚甲基蓝(MB)溶液作为液体废物测试模型来确定光催化能力。吸收器EM的稳定退火温度为900摄氏度,对于光催化施用是500℃。在该研究中,在稳定Fe3O4-Ac纳米粒子的性能和液体中的多功能复合材料的性能方面表明温度发挥着重要作用废物净化催化剂。 (c)2019年日本粉末技术学会。由elsevier b.v发表。和日本粉末科技会。版权所有。

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