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Synthesis of Geikielite (MgTiO3) Nanoparticles via Sol-Gel Method and Studies on Their Structural and Optical Properties

机译:溶胶-凝胶法合成Geikielite(MgTiO3)纳米粒子及其结构和光学性质的研究

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The geikielite (MgTiO3) ceramic nanoparticles with different compositions were synthesized by sol-gel method (termed as MT00, MT37, MT55, MT73, and MT100). The structural properties and average crystallite size were analysed. The results of Fourier transform infrared spectra for geikielite nanoparticles showed the presence of functional groups of -O-Ti-O-Mg-O-. The specific surface area of prepared nanoparticles surface area analyzer, which varied from 99 to 142 m(2)g(-1) for different compositions. The geikielite nanoparticles were transparent in the visible spectra region and revealed a sharp absorption edges at different wavelengths between 363 and 376 nm. The energy bandgap values of the nanostructured geikielites were investigated from the observed wavelength (i.e., from 3.38 to 3.53 eV). From the above observation, it can be concluded that the geikielite nanoparticles are the potential candidate for technological applications like dye synthesis solar cells and textiles for production.
机译:通过溶胶-凝胶法(称为MT00,MT37,MT55,MT73和MT100)合成了具有不同组成的Geikielite(MgTiO3)陶瓷纳米粒子。分析了结构性能和平均微晶尺寸。 Geikielite纳米粒子的傅立叶变换红外光谱结果表明,存在-O-Ti-O-Mg-O-官能团。制备的纳米颗粒表面积分析仪的比表面积,对于不同的成分,从99到142 m(2)g(-1)不等。 geikielite纳米粒子在可见光谱区域内是透明的,并且在363至376 nm之间的不同波长处显示出清晰的吸收边缘。从观察到的波长(即3.38至3.53eV)研究了纳米结构的geikielite的能带隙值。从以上观察结果可以得出结论,Geikielite纳米粒子是染料合成太阳能电池和生产纺织品等技术应用的潜在候选者。

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