H2O2/SOCl2: a useful reagent system for the conversion of thiocarbonyls to carbonyl compounds

Bahrami K; Khodaei MM; Farrokhi A

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H2O2/SOCl2: a useful reagent system for the conversion of thiocarbonyls to carbonyl compounds

机译：H2O2 / SOCl2：用于将硫代羰基转化为羰基化合物的有用试剂系统

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The H2O2/SOCl2 reagent system has been used as a new and efficient reagent for deprotection of thiocarbonyls to carbonyl compounds. The salient features of this protocol are short reaction times, good chemoselectivity, clean reaction profiles, and simple work-up that preclude the use of toxic solvents.

机译：H2O2 / SOCl2试剂系统已被用作将硫羰基脱保护为羰基化合物的新型高效试剂。该方案的显着特征是反应时间短，化学选择性好，反应曲线干净，后处理简单，可避免使用有毒溶剂。

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《Tetrahedron》 |2009年第36期|共4页
作者
Bahrami K; Khodaei MM; Farrokhi A;
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正文语种 eng
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MICROWAVE IRRADIATION; ORGANOPHOSPHORUS COMPOUNDS; OXIDATIVE AMIDATION; SELECTIVE OXIDATION; HYDROGEN-PEROXIDE; EFFICIENT METHOD; AMIDES; ALDEHYDES; TRANSFORMATION; THIOKETONES;

机译：微波辐照;有机磷化合物;氧化酰胺;选择性氧化;过氧化氢;高效方法;酰胺;醛;转化;硫酮;

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1. H2O2/SOCl2: a useful reagent system for the conversion of thiocarbonyls to carbonyl compounds [J] . Bahrami K, Khodaei MM, Farrokhi A Tetrahedron . 2009,第36期

机译：H2O2 / SOCl2：用于将硫代羰基转化为羰基化合物的有用试剂系统
2. Selective conversion of C=N bonds to their corresponding carbonyl compounds by the tribromoisocyanuric acid/wet SiO2 system as a novel reagent [J] . Davood Habibi, Mohammad Ali Zolfigol, Ali Reza Faraji Monatshefte fur Chemie . 2012,第5期

机译：三溴异氰尿酸/湿SiO2系统将C = N键选择性转化为其相应的羰基化合物作为新型试剂
3. EFFICIENT OXIDATIVE CONVERSION OF OXIMES TO THE CORRESPONDING CARBONYL COMPOUNDS WITH THE JONES REAGENT SUPPORTED ON GRAPHITE UNDER HETEROGENEOUS CONDITIONS [J] . JI-DONG LOU, FANG LIN, XIU LIAN LU Oxidation Communications . 2011,第3期

机译：在异质条件下，有效的氧化转化为石墨上支持的琼脂试剂的相应的羰基化合物
4. The use of hydrazine based derivatisation reagents for improved sensitivity and detection of carbonyl containing compounds "on tissue" using MALDI-MS [C] . Bryn Flinders, Peter S. Marshall, Josie Morrell, American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2010

机译：使用肼基衍生化试剂改善了使用MALDI-MS的含含肼的敏感性和检测“组织”的羰基化合物
5. PREPARATION OF BETA- TRIALKYLSTANNYL- ALPHA,BETA-UNSATURATED CARBONYL COMPOUNDS AND THEIR CONVERSION TO VINYLLITHIUM REAGENTS. [D] . MORTON, HOWARD ERIC. 1981

机译：β-三烷基苯乙烯基-α-羟基，β-不饱和的羰基化合物的制备及其转化为乙烯基LL试剂。
6. Disparate Behavior of Carbonyl and Thiocarbonyl Compounds: Acyl Chlorides vs Thiocarbonyl Chlorides and Isocyanates vs Isothiocyanates [O] . Kenneth B. Wiberg, Yi-gui Wang, Scott J. Miller, -1

机译：酰氯Vs硫羰基氯化物和异氰酸酯Vs异硫氰酸盐：羰基和硫代羰基化合物的不同行为
7. Carbon-13 nuclear magnetic resonance spectra of organic sulfur compounds. Comparison of chemical shifts for carbonyl and thiocarbonyl compounds in the pyrone, thiopyrone, and pyridone series [O] . I. W. J. Still, N. Plavac, D. M. McKinnon, 1976

机译：有机硫化合物的碳-13核磁共振光谱。羰基和硫代羰基化合物的化学位移比较吡喃酮，硫代酮和吡啶酮系列

H2O2/SOCl2: a useful reagent system for the conversion of thiocarbonyls to carbonyl compounds

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