Gas chromatographic determination of phosphorous and phosphoric acid chlorides in thionyl chloride

I. N. Stankov; S. N. Tarasov; V. S. Polyakov

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Gas chromatographic determination of phosphorous and phosphoric acid chlorides in thionyl chloride

机译：气相色谱法测定亚硫酰氯中的磷和磷酰氯

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A procedure was developed for the determination of trace amounts of phosphoric and phosphorous acid chlorides in reaction mixtures and commercial thionyl chloride. Samples were treated with a 1000-fold amount of ethanol, and phosphoric and phosphorous acid triesters were analyzed by gas chromatography using a thermionic detector.

机译：开发了一种测定反应混合物和市售亚硫酰氯中痕量磷和亚氯酰氯的方法。用1000倍量的乙醇处理样品，并使用热电子检测器通过气相色谱法分析磷酸和亚磷酸三酯。

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《Журнал аналитической химии》 |1999年第2期|共3页
作者
I. N. Stankov; S. N. Tarasov; V. S. Polyakov;
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正文语种 rus
中图分类分析化学;
关键词
gas chromatographic determination; phosphoric acid chlorides; phosphorous acid chlorides; thionyl chloride;

机译：气相色谱法;磷酰氯;亚磷酰氯;亚硫酰氯;

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1. Gas chromatographic determination of phosphorous and phosphoric acid chlorides in thionyl chloride [J] . I. N. Stankov, S. N. Tarasov, V. S. Polyakov Журнал аналитической химии . 1999,第2期

机译：气相色谱法测定亚硫酰氯中的磷和磷酰氯
2. Gas-chromatographic determination of sulfur dioxide, hydrogen chloride, and chlorine in thionyl chloride [J] . I. N. Stankov, S. N. Tarasov, V. S. Polyakov Журнал аналитической химии . 1999,第5期

机译：气相色谱法测定亚硫酰氯中的二氧化硫，氯化氢和氯
3. Gas-chromatographic determination of sulfur dioxide, hydrogen chloride, and chlorine in thionyl chloride [J] . I. N. Stankov, S. N. Tarasov, V. S. Polyakov Журнал аналитической химии . 1999,第5期

机译：天然气色谱法测定亚硫酰氯中二氧化硫，氯化氢和氯
4. Dehydration of N-Substitution Maleamic Acids with Thionyl Chloride [C] . C.Gaina, V. Gaina 12th Romanian International Conference on Chemistry and Chemical Engineering Sep 13-15, 2001 Bucharest, Romania . 2001

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5. Asymmetric synthesis of Calpha-methyl- gamma- and delta-amino acids from a common synthon and evaluation of thionyl chloride assisted peptide esterifications. [D] . Vogel, Emily Rose. 2015

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Gas chromatographic determination of phosphorous and phosphoric acid chlorides in thionyl chloride

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