A convenient method for ~(14)C-labeling of N-(2-oxo-5-phenyl-2,3- dihydro-1H-benzo[e][1,4]diazepin-3-yl)-1H-pyrrole-2-carboxamide-[carboxy- ~(14)C] as CCK-A antagonist

Saemian N.; Shirvani G.

首页> 外文期刊>Journal of Radioanalytical and Nuclear Chemistry: An International Journal Dealing with All Aspects and Applications of Nuclear Chemistry >A convenient method for ~(14)C-labeling of N-(2-oxo-5-phenyl-2,3- dihydro-1H-benzo[e][1,4]diazepin-3-yl)-1H-pyrrole-2-carboxamide-[carboxy- ~(14)C] as CCK-A antagonist

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A convenient method for ~(14)C-labeling of N-(2-oxo-5-phenyl-2,3- dihydro-1H-benzo[e][1,4]diazepin-3-yl)-1H-pyrrole-2-carboxamide-[carboxy- ~(14)C] as CCK-A antagonist

机译：N-（2-氧代-5-苯基-2,3-二氢-1H-苯并[e] [1,4]二氮杂-3-基）-1H-吡咯的〜（14）C标记的简便方法-2-羧酰胺-[羧基-〜（14）C]作为CCK-A拮抗剂

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N-(2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl) -1H-pyrrole-2-carboxamide-[carboxy- ~(14)C] was prepared as part of a five-step sequence from pyrrol-2-carbonitrile-[cyano- ~(14)C] as a key synthetic intermediate which has been synthesized from 2-bromopyrrole and zinc [~(14)C]-cyanide in the presence of tetrakis (triphenylphosphine) palladium.

机译：N-（2-氧代-5-苯基-2,3-二氢-1H-苯并[e] [1,4]二氮杂-3-基）-1H-吡咯-2-羧酰胺-[羧基-〜（14） [C]是由吡咯-2-腈-[氰基-〜（14）C]作为五步序列的一部分，它是由2-溴吡咯和锌[〜（14）C]合成的关键合成中间体四（三苯基膦）钯存在下的氰化物。

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《Journal of Radioanalytical and Nuclear Chemistry: An International Journal Dealing with All Aspects and Applications of Nuclear Chemistry》 |2012年第1期|共4页
作者
Saemian N.; Shirvani G.;
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正文语种 eng
中图分类物理化学（理论化学）、化学物理学;
关键词
3-Substituted 1; 4-benzodiazepine; Carbon-14; Cholecystokinin antagonist;

机译：3-取代的1;4-苯并二氮杂;碳14;胆囊收缩素拮抗剂;

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1. A convenient method for ~(14)C-labeling of N-(2-oxo-5-phenyl-2,3- dihydro-1H-benzo[e][1,4]diazepin-3-yl)-1H-pyrrole-2-carboxamide-[carboxy- ~(14)C] as CCK-A antagonist [J] . Saemian N., Shirvani G. Journal of Radioanalytical and Nuclear Chemistry: An International Journal Dealing with All Aspects and Applications of Nuclear Chemistry . 2012,第1期

机译：N-（2-氧代-5-苯基-2,3-二氢-1H-苯并[e] [1,4]二氮杂-3-基）-1H-吡咯的〜（14）C标记的简便方法-2-羧酰胺-[羧基-〜（14）C]作为CCK-A拮抗剂
2. Synthesis of carbon-~(14) analogue of N-(l-methyl-2-oxo-5-phenyl-2,3-dihydro-lH-benzo[e][l,4]diazepin-3-yl)-benzamide-[carboxyl-~(14)C] as CCK-A antagonist [J] . Nader Saemian, Gholamhossein Shirvani, Hojatollah Matloubi Journal of Labelled Compounds and Radiopharmaceuticals . 2006,第1期

机译：N-（1-甲基-2-氧代-5-苯基-2,3-二氢-1H-苯并[e] [l，4]二氮杂-3-基）苯甲酰胺的碳-（14）类似物的合成-[羧基-〜（14）C]作为CCK-A拮抗剂
3. A convenient method for ~(14)C-labeling of 2-methylthio-1-[4-N- α-ethoxycarbonylbenzyl)-amino-benzyl]-5-hydroxymethyl-2-[~(14)C]-1H-imidazole and 1-[4-N-α-ethoxy-carbonylbenzyl)- aminobenzyl]-5-hydroxymethyl-2-[~(14)C]-1H-imidazole as potential antihypertensives [J] . Saemian N., Shirvani G., Oliyaee S.S., Journal of Radioanalytical and Nuclear Chemistry: An International Journal Dealing with All Aspects and Applications of Nuclear Chemistry . 2012,第1期

机译：〜（14）C标记2-甲硫基-1- [4-N-α-乙氧基羰基苄基]-氨基-苄基] -5-羟甲基-2- [〜（14）C] -1H-咪唑的简便方法和1- [4-N-α-乙氧基-羰基苄基）-氨基苄基] -5-羟甲基-2- [〜（14）C] -1H-咪唑作为潜在的降压药
4. Synthesis of N-(2,3-dihydro-1-~14Cmethyl-2-oxo-5-phenyl-1H-1,4-benzodiazepin-3-yl)-benzamide and N-(2,3-dihydro-l-~14Cmethyl-2-oxo-5-phenyl-1H-1,4-benzodiazepin-3-yl) - N -~14C methyl-benzamide as novel carbon-14 labelled CCK Antagonists [C] . Gholamhossein Shirvani, Hojatollah Matloubi Nader Saemian International Conference on Isotopes (5ICI) . 2005

机译：N-（2,3-二氢-1- 〜14℃甲基-2-氧代-5-苯基-1H-1,4-苯并二氮哌己嘧啶-3-基-3-基（2,3-二氢）的合成-1- 〜14c甲基-2-氧代-5-苯基-1H-1,4-苯并二氮嘧啶-3-基） - N - 〜14C甲基 - 苯甲酰胺作为新型碳-14标记的CCK拮抗剂
5. tert-Butyl N-{3-(3-chloro-14-dioxo-14-dihydronaphthalen-2-yl)aminopropyl}carbamate [O] . Jackson A. L. C. Resende, Javier A. Gomez 2012

机译：N- {3-（3-氯-14-二氧杂-14-二氢萘-2-基）氨基丙基}氨基甲酸叔丁酯
6. Crystal structure of N-[(8E)-12-methyl-14-phenyl-10,13,14,16-tetraazatetracyclo[7.7.0.02,7.011,15]hexadeca-1(16),2,4,6,9,11(15),12-heptaen-8-ylidene]hydroxylamine 1,4-dioxane hemisolvate [O] . Shaaban K. Mohamed, Joel T. Mague, Mehmet Akkurt, 2015

机译：N - [（8E）-12-甲基-14-苯基-10,13,14,16-四氮杂四环[7.7.0.02,7.011,15]十六碳-1（16），2,4,6,9的晶体结构，11（15），12-庚烯-8-亚基]羟胺1,4-二恶烷半溶剂化物

A convenient method for ~(14)C-labeling of N-(2-oxo-5-phenyl-2,3- dihydro-1H-benzo[e][1,4]diazepin-3-yl)-1H-pyrrole-2-carboxamide-[carboxy- ~(14)C] as CCK-A antagonist

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