Synthesis of methyl-2,4-bis(cyclohexane)dispiro-1,2,3,4,4a,5,6,7-octahydro-(1H,3H)quinazoline-8-carbodithioate derived from cyclohexanone in one step

Ricardo R.Contreras; Bernardo Fontal; Ali Bahsas; Marisela Reyes; Trino Suarez; Fernando Bellandi

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Synthesis of methyl-2,4-bis(cyclohexane)dispiro-1,2,3,4,4a,5,6,7-octahydro-(1H,3H)quinazoline-8-carbodithioate derived from cyclohexanone in one step

机译：一步法合成环己酮衍生的2,4-双（环己烷）二螺甲基1,1,2,3,4,4a，5,6,7-八氢-（1H，3H）喹唑啉-8-碳二硫酸酯

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The new compound methyl-2,4-bis(cyclohexane)dispiro-1,2,3,4,4a,5,6,7-octahydro-(1H,3H)-quinazoline-8-carbodithioate has been synthesized from cyclohexanone and carbon disulfide. In has been characterized by uv-visible, FTIR, mass spectra and a complete structure based on ~1H and ~(13)C NMR spectroscopy.

机译：由环己酮和环己酮合成了新的化合物2,2,4-双（环己烷）二螺甲基1,2,3,4,4a，5,6,7-八氢-（1H，3H）-喹唑啉-8-碳二硫代酸酯二硫化碳。 In具有紫外可见光谱，FTIR，质谱和基于〜1H和〜（13）C NMR光谱的完整结构的特征。

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《Journal of Heterocyclic Chemistry: The International Journal of Heterocyclic Chemistry》 |2001年第5期|共3页
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Ricardo R.Contreras; Bernardo Fontal; Ali Bahsas; Marisela Reyes; Trino Suarez; Fernando Bellandi;
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1. Synthesis of methyl-2,4-bis(cyclohexane)dispiro-1,2,3,4,4a,5,6,7-octahydro-(1H,3H)quinazoline-8-carbodithioate derived from cyclohexanone in one step [J] . Ricardo R.Contreras, Bernardo Fontal, Ali Bahsas, Journal of Heterocyclic Chemistry: The International Journal of Heterocyclic Chemistry . 2001,第5期

机译：一步法合成环己酮衍生的2,4-双（环己烷）二螺甲基1,1,2,3,4,4a，5,6,7-八氢-（1H，3H）喹唑啉-8-碳二硫酸酯
2. Synthesis and Crystal Structure of 1,6:3,4-Bis(1,2-xylyiene) tetrahydro-imidazo4,5-dimidazole-2,5(1H,3H)-dione [J] . LIU Hongxia, CAI Wei, LI Qiong 半导体光子学与技术（英文版） . 2010,第004期
3. Shaken not stirred: a facile synthesis of 1,4-bis(furo(2,3-d)-pyrimidine-2,4(1H,3H)-dione-5-yl)benzenes by one-pot reaction of isocyanides, N,N'-dimethylbarbituric acid, and terephthaldialdehyde. [J] . Teimouri MB, Bazhrang R Bioorganic and Medicinal Chemistry Letters . 2006,第14期

机译：不摇晃不摇：通过一锅异氰酸酯N反应轻松合成1,4-双（呋喃（2,3-d）-嘧啶-2,4（1H，3H）-二酮-5-基）苯，N'-二甲基巴比妥酸和对苯二醛。
4. Pyrimidine Derivatives. VIII. One-Step Synthesis of 3,4-Dihydro-pyrimido(6,1-c)(1,4)oxazine Derivatives by Reactions of 5-Bromo-1-(2-bromoethyl)-6-bromomethyl-2,4(1H,3H)-pyrimidinedione with Sodium Alkoxides and 2-Nitropropane. [O] . Toshio KINOSHITA, Miho UGA, Youko TANIMOTO, 1992

机译：嘧啶衍生物。 VIII。通过5-溴-1-（2-溴乙基）-6-溴甲基-2,4的反应，通过反应进行3,4-二氢嘧啶（6,1-C）（1,4）恶嗪衍生物的一步合成（1,4）恶嗪衍生物（1小时，3h） - 用醇钠和2-硝基丙烷吡啶氧二氧化硫。

Synthesis of methyl-2,4-bis(cyclohexane)dispiro-1,2,3,4,4a,5,6,7-octahydro-(1H,3H)quinazoline-8-carbodithioate derived from cyclohexanone in one step

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