SYNTHESIS OF PYRROLOAZEPINES - FACILE SYNTHESIS OF 2-SUBSTITUTED PYRROLE DERIVATIVES BY THE PHOSGENE METHOD

Cho H.; Mizuno A.; Annoura H.; Tatsuoka T.; Matsuki S.

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SYNTHESIS OF PYRROLOAZEPINES - FACILE SYNTHESIS OF 2-SUBSTITUTED PYRROLE DERIVATIVES BY THE PHOSGENE METHOD

机译：光气法合成吡咯并庚烯-2-取代吡咯衍生物的脂肪酸合成。

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A highly convenient method for the synthesis of 2-substituted pyrrole derivatives 7a-c from pyrrole using phosgene was developed. Successively, 7-methyl-6,7-dihydro-1H,5H-pyrrolo[2,3-c]azepine-4,8-dione 1a and 6,7-dihydro-1H,5H-pyrrolo[2,3-c]azepine-4,8-dione 1b (aldisin) were synthesized by phosphorus pentoxide/methanesulfonate and polyphosphoric acid cyclization. [References: 10]

机译：开发了一种使用光气从吡咯合成2-取代的吡咯衍生物7a-c的非常方便的方法。依次为7-甲基-6,7-二氢-1H，5H-吡咯并[2,3-c]氮杂-4,8-二酮1a和6,7-二氢-1H，5H-吡咯并[2,3-c通过五氧化二磷/甲磺酸根和多磷酸环化合成] azepine-4,8-dione 1b（aldisin）。 [参考：10]

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《Journal of Heterocyclic Chemistry: The International Journal of Heterocyclic Chemistry》 |1997年第1期|共5页
作者
Cho H.; Mizuno A.; Annoura H.; Tatsuoka T.; Matsuki S.;
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正文语种 eng
中图分类有机化学;
关键词
Marine natural-products;

机译：海洋天然产物;

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1. SYNTHESIS OF PYRROLOAZEPINES - FACILE SYNTHESIS OF 2-SUBSTITUTED PYRROLE DERIVATIVES BY THE PHOSGENE METHOD [J] . Cho H., Mizuno A., Annoura H., Journal of Heterocyclic Chemistry: The International Journal of Heterocyclic Chemistry . 1997,第1期

机译：光气法合成吡咯并庚烯-2-取代吡咯衍生物的脂肪酸合成。
2. Oxidation Strategy for the Synthesis of Regioisomeric Spiroisobenzofuranopyrroles: Facile Entries to Spiro[isobenzofuran-1,2 '-pyrrole] and Spiro[isobenzofuran-1,3 '-pyrrole] Derivatives [J] . Fan Yefeng, Liu Song, Chen Nanyang, Synlett . 2015,第3期

机译：区域异构的螺异苯并呋喃并吡咯的氧化策略：螺[异苯并呋喃-1,2'-吡咯]和螺[异苯并呋喃-1,3'-吡咯]衍生物的容易入口
3. Synthesis of 2,3,4-trisubstituted pyrrole derivatives via [3+2] cyclization of activated methylene isocyanides with 4-(arylidene)-2-substituted oxazol-5(4H)-ones [J] . Organic Chemistry Frontiers . 2020,第2期

机译：用4-（亚亚亚胺）-2-取代的恶唑-5（4H）环化活化亚甲基异氰化物的6,4-三取代的吡咯衍生物的合成氧化酯的环化
4. An efficient synthesis of 2-substituted pyrrole stable phosphorus ylides from reaction between pyrrole and acetylenic esters in the presence of triphenylphosphine in water-acetone media(Abstracts) [C] . Malek Taher Maghsoodlou, Nourollah Hazeri, Sayyed Mostafa Habibi Khorassani European Symposium on Organic Chemistry . 2007

机译：在水 - 丙酮培养基中的三苯基膦（摘要）中，在吡咯和乙炔酯之间的2取代吡咯稳定磷ylides中的高效合成。
5. Green chemistry in pyrrole synthesis. I. Solvent effect in Barton-Zard pyrrole synthesis: An improved synthesis of 3,4-dialkyl-1H-pyrrole-2-carboxylates. II. A novel route for the synthesis of pharmaceutically important pyrrole derivatives. [D] . Cherukuri, Sankara R. 2005

机译：吡咯合成中的绿色化学。 I.Barton-Zard吡咯合成中的溶剂作用：3，4-二烷基-1H-吡咯-2-羧酸酯的改进的合成。二。合成重要的吡咯衍生物的新途径。
6. A Facile Mild And Efficient One-Pot Synthesis of 2-Substituted Indole Derivatives Catalyzed By Pd(PPh3)2Cl2 [O] . Hossien A. Oskooie, Majid M. Heravi, Farahnaz K. Behbahani 2007

机译：Pd（PPh3）2Cl2催化的2取代吲哚衍生物的快速轻巧高效一锅合成
7. Facile Synthesis of 2,3-Disubstituted Pyrroles from 2-Substituted 1-Pyrrolines [O] . Mitsunori Oda, Yurie Fujiwara, Taku Shoji, 2012

机译：从2取代的1-吡咯的2,3-二取代的胃肠杆菌的体面合成

SYNTHESIS OF PYRROLOAZEPINES - FACILE SYNTHESIS OF 2-SUBSTITUTED PYRROLE DERIVATIVES BY THE PHOSGENE METHOD

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