SYNTHESIS OF FUNCTIONALISED BICYCLO[4.4.0] AND SPIRO[5.4] COMPOUNDS BY TIN-MEDIATED RADICAL CYCLIZATION

Shanmugam P.; Rajagopalan K.; Srinivasan R.

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SYNTHESIS OF FUNCTIONALISED BICYCLO[4.4.0] AND SPIRO[5.4] COMPOUNDS BY TIN-MEDIATED RADICAL CYCLIZATION

机译：锡介导的自由基循环合成功能化双环[4.4.0]和螺[5.4]化合物

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Functionalised bicyclo[4.4.0] system 5, and spiro[5.4] system 10 were synthesised from the bispropargyl compound 3 and the monopropargyl compound 6 by tin-mediated radical cyclization. (C) 1997 Elsevier Science Ltd. [References: 20]

机译：通过锡介导的自由基环化反应，由双炔丙基化合物3和单炔丙基化合物6合成了功能化的双环[4.4.0]系统5和螺[5.4]系统10。（C）1997 Elsevier Science Ltd. [参考：20]

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《Tetrahedron》 |1997年第34期|共8页
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Shanmugam P.; Rajagopalan K.; Srinivasan R.;
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正文语种 eng
中图分类有机化学;
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Stereocontrolled synthesis; Systems;

机译：立体合成;系统;

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1. SYNTHESIS OF FUNCTIONALISED BICYCLO[4.4.0] AND SPIRO[5.4] COMPOUNDS BY TIN-MEDIATED RADICAL CYCLIZATION [J] . Shanmugam P., Rajagopalan K., Srinivasan R. Tetrahedron . 1997,第34期

机译：锡介导的自由基循环合成功能化双环[4.4.0]和螺[5.4]化合物
2. Synthesis of carbo- and aza-bicyclo[4.3.0] and [4.4.0] compounds by Ti(II)-mediated cyclization of 2,7- or 2,8-enynyl-1-ol derivatives [J] . Yongcheng Song, Sentaro Okamoto, Fumie Sato Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2002,第37期

机译：Ti（II）介导的2,7-或2,8-炔基-1-醇衍生物的环化反应合成碳-和氮杂双环[4.3.0]和[4.4.0]化合物
3. Synthesis of carbo- and aza-bicyclo[4.3.0] and [4.4.0] compounds by Ti(II)-mediated cyclization of 2,7- or 2,8-enynyl-1-ol derivatives [J] . Yongcheng Song, Sentaro Okamoto, Fumie Sato Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2002,第37期

机译：Ti（II）介导的2,7-或2,8-炔基-1-醇衍生物的环化反应合成碳-和氮杂双环[4.3.0]和[4.4.0]化合物
4. Electrosynthesis of Heterocyclic Compounds by Radical Cyclization in Environmentally Friendly Media [C] . J.P. Mendes, J.M.S.S. Esperanca, A.P. Esteves, Mechanistic organic electrochemistry . 2015

机译：在环境友好的介质中通过自由基环化电合成杂环化合物
5. Exploratory studies in free radical chemistry: Chapter 1. Use of bis(cyclopentadienyl)titanium(III) chloride as a single electron reductant. Chapter 2. Titanium(III) mediated pent-4-enyl radical cyclizations. Chapter 3. Tributyltin mediated hept-6-enyl radical cyclizations: Synthesis of thionocarbonates and thiocarbamates. [D] . Bliss, Brian Irving Alban. 2000

机译：自由基化学的探索性研究：第1章。氯化双（环戊二烯基）钛（III）作为单电子还原剂的用途。第2章。钛（III）介导的戊4烯基自由基环化。第3章。三丁基锡介导的庚6-烯基自由基环化：硫代碳酸酯和硫代氨基甲酸酯的合成。
6. Synthesis of Conformationally-Locked cis- and trans-Bicyclo4.4.0 Mono- Di- and Trioxadecane Modifications of Galacto- and Glucopyranose. Experimental Limiting 3JHH Coupling Constants for the Estimation of Carbohydrate Side Chain Populations and Beyond [O] . Harsha Amarasekara, Suresh Dharuman, Takayuki Kato, -1

机译：构型锁定的顺式和反式双环4.4.0半乳糖和葡糖醛糖的单双和三氧十二烷修饰基团的合成。估计侧链碳原子及以上的实验极限3JHH耦合常数
7. Synthesis of optically pure 3-(1n.pi.*)-(1S,6R)-bicyclo[4.4.0]decane-3,8-dione, a molecule which is chiral in the excited state only [O] . Miesen, FWAM Sjoerd, Wollersheim, APP, Meskers, SCJ Stefan, 1994

机译：光学纯的3-（1n.pi。*）-（1S，6R）-双环[4.4.0]癸烷-3,8-二酮的合成，该分子仅在手性处于激发态
8. Heptacyclo(5.5.1.14,10.02,6.03,11.05,9.08,12)tetradecane-13,14- bis(spiro-1 prime-cyclopentane): A New C22H28 Nonacyclic Cage Hydrocarbon. Improved Synthesis Bicyclo(2.2.1)hepta-2,5-diene-7-spiro-1 prime-cyclo-pentane [R] . Marchand, A. P., Wu, A. H. 1985

机译：Heptacyclo（5.5.1.14,10.02,6.03,11.05,9.08,12）十四烷-13,14-双（螺-1-环戊烷）：新的C22H28非环状笼烃。改进的合成双环（2.2.1）七-2,5-二烯-7-螺-1-原 - 环 - 戊烷

SYNTHESIS OF FUNCTIONALISED BICYCLO[4.4.0] AND SPIRO[5.4] COMPOUNDS BY TIN-MEDIATED RADICAL CYCLIZATION

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