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Characterization of Some Jordanian Crude and Exhausted Olive Pomace Samples

机译:一些约旦原油和精制橄榄果渣样品的表征

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In an attempt to provide a set of specifications for the use and trade of the olive pomace in Jordan, several samples of the crude and laboratory-prepared exhausted (oil-free) olive pomace have been subjected to a thorough thermochemical characterization. Such characterization included determination of fat content by using n-hexane and Soxhlet extractor, ultimate and proximate analyses obtained by using an elemental analyzer and a thermogravimetric procedure, respectively, gross and net calorific values obtained by using adiabatic oxygen bomb calorimetry, mineral content (ash), and analysis of the pyrolysis thermograms in terms of specified temperatures and residual masses associated with such temperatures as obtained under an inert atmosphere of nitrogen gas at a flow rate of 100 ml per min and a heating rate of 20°C per min from room temperature up to 600°C. The properties of both the crude and the exhausted olive pomace were compared. The gross calorific values and the results of the ultimate analyses for the two pomace types were found to correlate very well as indicated by the use of a literature correlation formula usually used for estimating the gross calorific value of a fuel when its ultimate analysis is known. Other literature correlation formulas used for estimating the gross calorific value from the proximate analysis data were also used to check the adequacy of our procedure for getting the proximate analysis from the?thermogravimetric pyrolysis thermograms.
机译:为了为约旦的橄榄果渣的使用和贸易提供一套规范,已对一些粗制和实验室准备的废(无油)橄榄果渣样品进行了彻底的热化学表征。此类表征包括使用正己烷和索氏提取器测定脂肪含量,分别通过元素分析仪和热重分析程序获得的最终和最接近分析,通过绝热氧弹量热法获得的总和净热值,矿物质含量(灰分) ),并根据规定的温度和与此类温度相关的残余质量分析热解热分析图,这些温度是在氮气惰性气氛下以每分钟100 ml的流速和每分钟20°C的加热速率在室温下获得温度高达600°C。比较了粗制和用尽的橄榄果渣的性能。发现这两种果渣类型的总热值和最终分析的结果之间具有很好的相关性,这是通过使用文献相关公式得出的,该公式通常用于在已知燃料的最终分析时估算燃料的总热值。用于从近似分析数据估算总热值的其他文献相关公式也用于检查我们从热解热解热分析图获得近似分析的程序是否足够。

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