通过Suzuki偶联反应合成了4-溴-2-硝基联苯,对反应条件进行了优化选择,研究了反应温度、反应时间、反应所需用的碱对反应收率的影响,并通过气相色谱、液相色谱、红外、核磁、气质联用对得到的目标产物进行了表征分析。%In this paper,4-Bromo-2-nitro-biphenyl had been synthesized by Suzuki coupling. The reaction conditions, such as temperature,time and base used in the reaction,were investigated,and the product was characterized and analyzed by HPLC,IR,NMR and GC-MS.
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