Synthesis and Crystal Structure of （E）-4-（3-oxo-3-（（4- （N-（pyrimidin-2-yl）-sulfamoyl）phenyl）amino）prop- 1-en-l-yl）-l,2-phenylene diacetate Dimethanol

摘要

The title compound, (E)-4-(3-oxo-3-((4-(N-(pyrimidin-2-yl)sulfamoyl)-phenyl)ami- no)prop- 1-en- 1-yl)- 1,2-phenylene diacetate dimethanol, was synthesized by the reaction of caffeic acid with sulfadiazine and characterized by FT-IR, 1H-NMR spectroscopy, ESI-MS and X-ray single-crystal diffraction. It crystallizes in triclinic, space group P1 with a = 10.302(7), b = 11.621(8), c = 12.107(8)A, a = 100.904(9), β = 102.624(8), y = 95.501(9)°, V= 1374.5(15)A3, Z= 2, F(000) = 588, D,= 1.354 Mg/m3, Mr = 560.57,μ= 0.176 mm-1, 2 = 0.71073 A, the final R = 0.0666 and wR = 0.1950 for 4774 observed reflections with I 〉 2σ(I).