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Synthesis of CuFe_2O_4-Bentonite Composite for Adsorption of Ni(II) from Electroplating Wastewater

机译:CuFe_2O_4-膨润土复合材料的合成,用于吸附Ni(II)电镀废水

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CuFe_2O_4-bentonite composite successfully synthesized using chemical co-precipitation method and using to adsorp Ni(II) from electroplating wastewater. The composite was characterized by Fourier Transform Infra Red and Scanning Electron Microscope-Energy Dispersive X Ray Spectroscopy. The FTIR spectra of CuFe2O_4-bentonite composite presented the characteristic of CuFe_2O_4 and bentonite. Typical of bentonite obtained by the bands at 1033.8 cm~(-1) correspondent to the intensity of Si-O. The observed two peaks at 432.0 cm"1 and 536.2 cm~(-1) attributed to the tetrahedral and octahedral of CuFe_2O_4. The result indicated that CuFe_2O_4 particles deposited on the surface of bentonite. The main component of CuFe_2O_4-bentonite composite contained of CuFe_2O_4 and bentonite from EDX spectra. Batch experiments were carried out to investigate optimum condition of adsorption Ni(II) onto CuFe_2O_4-bentonite composite. The optimum condition for initial concentration of Ni(II) 50 mg L~(-1) and volume 50 mL obtained at weight of CuFe_2O_4-bentonite composite of 100 mg, contact times at 60 minutes and pH of the solution 5. The adsorption efficiency of Ni(II) from electroplating wastewater using CuFe_2O_4-bentonite composite at optimum condition was 99.136 %, respectively.
机译:CuFe_2O_4膨润土复合使用化学共沉淀方法,用从电镀废水adsorp镍(II)成功合成。复合材料的特征在于傅里叶变换红外线红色和扫描电子显微镜 - 能量分散X射线光谱。 CuFe2O_4-膨润土复合物的FTIR光谱呈现了CuFe_2O_4和膨润土的特征。由1033.8cm〜(-1)的带状的典型膨润土对应于Si-O的强度。在432.0cm“1和536.2cm〜(-1)中观察到的两个峰,归因于Cufe_2O_4的四面体和八面体。结果表明Cufe_2O_4沉积在膨润土表面上的颗粒。Cufe_2O_4-膨润土复合材料的主要成分包含在Cufe_2O_4和从EDX光谱膨润土。分批实验进行研究到CuFe_2O_4膨润土吸附的最佳条件的Ni(II)复合物。最佳条件为镍的初始浓度(II)50毫克L〜(-1)和50体积毫升得到100mg的Cufe_2O_4-膨润土复合材料的重量,60分钟的接触时间和溶液的pH。Ni(ii)在最佳条件下使用Cufe_2O_4-膨润土复合材料电镀废水的吸附效率分别为99.136%。

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