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Characterization of oil based nanofluid for quench medium

机译:淬火介质油纳米流体的表征

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The choice of quench medium depends on the hardenability of the metal alloy, the thickness of the component, and the geometry of the component. Some of these will determine the cooling rate required to obtain the desired microstructure and material properties. Improper quench media will cause the material to become brittle, suffers from geometric distortion, or having a high undesirable residual stresses in the components. In heat treatment industries, oil and water are frequently used as the quench media. Recently, nanofluid as a quench medium has also been studied using several different fluids as the solvent. Examples of frequently used solvents include polymers, vegetable oils, and mineral oil. In this research, laboratory-grade carbon powder were used as nanoparticle. Oil was used as the fluid base in this research as the main observation focus. To obtain nanoscale carbon particles, planetary ball mill was used to ground laboratory grade carbon powder to decrease the particle size. This method was used to lower the cost for nanoparticle synthesis. Milling speed and duration were set at 500 rpm and 15 hours. Field Emission Scanning Electron Microscope (FE-SEM), and Energy Dispersive X-Ray (EDX) measurement were carried out to determine the particle size, material identification, particle morphology, and surface change of samples. The carbon nanoparticle content in nanofluid quench mediums for this research were varied at 0.1%, 0.2%, 0.3%, 0-4, and 0.5 % volume. Furthermore, these mediums were used to quench JIS S45C or AISI 1045 carbon steel samples which annealed at 1000°C. Hardness testing and metallography observation were then conducted to further examine the effect of different quench medium in steel samples.
机译:淬火介质的选择取决于金属合金的淬透性,组件的厚度和部件的几何形状。其中一些将确定获得所需微观结构和材料性能所需的冷却速率。不正确的淬火介质将导致材料变脆,遭受几何变形,或者在组件中具有高不希望的残余应力。在热处理行业中,油和水经常用作淬火介质。最近,还使用几种不同的流体作为溶剂研究了纳米流体作为骤冷培养基。经常使用的溶剂的实例包括聚合物,植物油和矿物油。在该研究中,实验室级碳粉用作纳米粒子。用作本研究中的流体基地作为主要观察重点。为了获得纳米级碳颗粒,用行星球磨机用于研磨实验级碳粉以降低粒度。该方法用于降低纳米粒子合成的成本。铣削速度和持续时间设定为500 rpm和15小时。进行现场发射扫描电子显微镜(Fe-SEM)和能量分散X射线(EDX)测量以确定样品的粒度,材料鉴定,颗粒形态和表面变化。该研究的纳米流体淬火介质中的碳纳米粒子含量为0.1%,0.2%,0.3%,0-4和0.5%体积。此外,这些培养基用于淬火JIS S45C或AISI 1045碳钢样品,其在1000℃下退火。然后进行硬度测试和金相观察以进一步检查不同淬火介质在钢样中的效果。

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