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The Effect of Extract Concentration of Diospyros discolor Willd. as Silver Nanoparticles Synthesis

机译:二旋气褪色剂萃取物浓度的影响。 作为银纳米粒子合成

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Diospyros discolor Willd. (Bisbul) is known to have an activity as a reducing agent to reduce silver ions into silver nanoparticles. These abilities affected by the phytochemical content in the extract, such as phenolics and flavonoids compounds, which makes the synthesis process to be environmentally friendly. In this study, various concentrations of crude water extract from Bisbul leaves were used at concentration 0.01, 0.025, and 0.05 % (w/v), with the ratio between the extract and 1 mM AgNO_3 was 1:9 (v/v). The formation of silver nanoparticles are confirmed by the presence of absorption spectra between 350-450 nm using UV-Vis spectrophotometer. Based on the results of phytochemical tests, it showed that the extract contains phenols and flavonoids compound. Furthermore, the total flavonoid content (TFC) and total phenolic content (TPC) were measured to know their presence in the extract. The amount of those compounds in each extract concentration tend to increase with the increasing of extract concentration. The extract with concentration 0.05 % had a narrower peak width based on the Full Width at Half Maximum (FWHM) value, which can indicate the monodispersity in silver nanoparticles size and distribution.
机译:Diospyros Discoloror Willd。已知(Bisbul)具有作为还原剂的活性,以将银离子还原成银纳米颗粒。这些能力受到提取物中植物化学含量影响的能力,例如酚类和黄酮化合物,这使得合成过程是环保的。在该研究中,在浓度0.01,0.025和0.05%(w / v)的浓度下使用各种浓度的粗水萃取物,提取物和1mM AgnO_3之间的比例为1:9(v / v)。通过使用UV-Vis分光光度计,通过350-450nm的吸收光谱的存在来确认银纳米颗粒的形成。基于植物化学测试的结果,表明提取物含有酚类和黄酮化合物。此外,测量总黄酮含量(TFC)和总酚含量(TPC)以了解它们在提取物中的存在。随着提取物浓度的增加,每种提取物浓度中的这些化合物的量趋于增加。浓度为0.05%的提取物的峰值宽度较窄,基于半最大(FWHM)值的全宽,这可以指示银纳米颗粒尺寸和分布中的单反叠性。

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