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The effects of crystallite structure LaMnO_3 nanoparticles on the adsorption of synthesized LaMnO_3/graphene composites

机译:微晶结构LAMNO_3纳米粒子对合成兰诺/石墨烯复合材料吸附的影响

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The LaMnO_3/graphene composites have been successfully synthesized using co-precipitation method at five different calcination temperature of LaMnO_3 nanoparticles (untreated, 500°C, 600°C, 700°C, and 800°C. The effects of calcination temperature on the formation of LaMnO_3 nanoparticles on LaMnO_3/graphene were investigated. The average grain size of LaMnO_3/graphene increases with increasing calcination temperature on LaMnO_3 nanoparticles. The use of calcination can effectively reduce the crystallization of LaMnO_3 nanoparticles on LaMnO_3/graphene composites. LaMnO_3/graphene shows the orthorhombic structure of LaMnO_3 nanoparticles while the peak of graphene cannot be identified owing to graphene's broad peak. The LaMnO_3 nanoparticles obtained at a calcination temperature of 800 °C exhibits superior adsorption to remove methylene blue. Furthermore, the adsorption test of methylene blue using LaMnO_3/graphene follows a pseudo-second order kinetic process and Langmuir model.
机译:已经在兰诺_3纳米颗粒的五种不同煅烧温度下使用共沉淀法(未处理,500℃,600℃,700℃和800℃,成功地合成了LamnO_3 /石墨烯复合材料。煅烧温度对形成的影响研究了Lamno_3纳米粒子上的兰诺_3 /石墨烯。兰诺_3 /石墨烯的平均晶粒尺寸随着兰诺_3纳米颗粒的煅烧温度的增加而增加。可以有效地降低兰诺_3纳米颗粒在兰诺_3 /石墨烯复合材料上的结晶。LAMNO_3 /石墨烯显示兰诺_3纳米粒子的正交结构,同时不能鉴定到石墨烯的宽峰的峰值。在800℃的煅烧温度下获得的兰诺_3纳米颗粒具有优异的吸附以除去亚甲基蓝色。此外,使用Lamno_3 /的亚甲基蓝色的吸附试验/石墨烯遵循伪二阶动力学工艺和Langmuir模型。

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