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Studies on degradation performance of Mg-4.0Zn-1.5Sr alloy with coated of the laser surface processing combining alkaline treatment

机译:碱性处理结合激光表面处理的Mg-4.0Zn-1.5SR合金的降解性能研究

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The surface modification of biomaterial Mg-4.0Zn-1.5Sr alloy has been done by means of laser surface processing combining alkaline treatment process, as well as the degradation performance of Mg-4.0Zn-1.5Sr alloy with and without coatings in Hank's solution has been analyzed comparatively. The results indicate that the optimal parameters of laser surface processing are that the power is 3 kW, the current 200 A, the width 1mm, the defocus amount 135 mm and the scanning speed 1mm/s. The optimal parameters of alkaline treatment are that the solution is NaOH, the concentration 0.5 mol/L, the temperature 80 °C and the time 12 h. There are only two phases of Mg (OH)2 and magnesium matrix, and the surface generated most of Mg (OH)2 which can improve the corrosion resistance of the alloy after laser combining alkaline treatment, as well as the corrosion rate is almost the stable, which is much smaller than both of uncoated and laser surface processing. The study of the electrochemical corrosion behavior shows that the corrosion potential of the alloy with coated of laser combining alkaline treatment is improved 0.1277 V than that of laser treatment, and the corrosion current is decreased 470.2 muA than laser treatment. The corrosion resistant ability of Mg-4.0Zn-1.5Sr alloy is greatly improved by means of laser combining alkaline treatment.
机译:已经通过混合碱性处理方法的激光表面处理来完成生物材料Mg-4.0Zn-1.5SR合金的表面改性,以及Hank解决方案中的Mg-4.0Zn-1.5SR合金的降解性能和没有涂层的涂层已经相对分析。结果表明,激光表面处理的最佳参数是功率为3 kW,电流200a,宽度1mm,散焦量135mm和扫描速度为1mm / s。碱性处理的最佳参数是溶液是NaOH,浓度0.5mol / L,温度80℃和12小时的时间。 Mg(OH)2和镁基质中只有两相,并且表面产生的大部分Mg(OH)2,其可以改善激光结合碱性处理后合金的耐腐蚀性,以及腐蚀速度几乎是腐蚀速率稳定,远小于无涂层和激光表面处理。电化学腐蚀行为的研究表明,具有激光组合碱性处理的合金的腐蚀电位得到0.1277V而不是激光处理,腐蚀电流比激光处理减少470.2μm。通过混合物组合碱性处理,Mg-4.0Zn-1.5SR合金的耐腐蚀性大大提高。

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