Magnetic nanomaterials with emergent physical and chemical properties have paid much attention, however, their synthesis pathways are still a challenge. In this study, we described a simple method for the synthesis of graphene oxide-decorated magnetic nanoparticles GO@MFe2O4 (M = cobalt, manganese and nickel metal sites) from ferrites MFe2O4 via complex polymerization method and graphene oxide via Hummer's method. The structure of GO@MFe2O4 were characterized by several physicochemical techniques, such as X-ray Diffraction (XRD) and Scanning electron microscope (SEM), Brunauer-Emmett-Teller (BET), point of zero charge (pH_(pzc)) and Fourier-transform infrared spectroscopy (FTIR). The results indicated a spinel-like structure of GO@MFe2O4 with high porosity and surface area, along with strong saturation magnetization, which can become a potential candidate for various applications.
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机译:具有紧急物理和化学性质的磁性纳米材料得到了很多关注,然而,它们的合成途径仍然是一个挑战。在该研究中,我们描述了通过蜂扣法通过复合聚合方法和石墨烯氧化物从铁氧烷MFE2O4合成石墨烯氧化物装饰磁性纳米颗粒GO @ MFE2O4(M =钴,锰和镍金属位点)的简单方法。 Go @ MFE2O4的结构的特征在于几种物理化学技术,例如X射线衍射(XRD)和扫描电子显微镜(SEM),Brunauer-Emmett-Teller(Bet),零电荷点(PH_(PH_(PCZC))和傅里叶变换红外光谱(FTIR)。结果表明,具有高孔隙率和表面积的GO @ MFE2O4的尖晶石结构,以及强饱和磁化强度,其可以成为各种应用的潜在候选者。
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