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Effect of nanoclay, Cloisite15A on the Mechanical Properties and Thermal behavior of Glass Fiber Reinforced Polyester

机译:纳米粘土,Cloisite15a对玻璃纤维增​​强聚酯机械性能和热行为的影响

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摘要

A series of glass fiber reinforced polyester nanocomposites have been prepared with varying compositions viz., 0, 0.5, 1, 1.5 and 2 wt % Cloisitel5A as nanofiller. . The effects of nanoclay content on the mechanical, dynamic mechanical and thermal properties of nanocomposites were studied. Tensile testing, Impact testing, Dynamic Mechanical Analysis and Thermogravimetric analysis are employed to investigate mechanical and thermal characteristics. Tensile and impact test results are pointing to the optimum percentage of clay loading as 1%. Also the Tensile modulus attains the optimum status at 1% filled samples for different Cross head speed (CHS). Dynamic mechanical behavior does not indicate any consistent behavior. However the storage modulus showed an improved performance for 1% nano filled sample. The glass Transition Temperature, T_g falls in the range 95 to 110 °C for all samples. Thermogravimetric Analysis indicates the first phase of degradation starts around 200 °C for all samples. The fractured surface analyzed by Scanning Electron Microscopy(SEM) indicate brittle nature of fracture for pure polyester reinforced with glass fiber mat, Whereas the fracture changed to ductile nature by the addition of nano clay.
机译:已经制备了一系列玻璃纤维增​​强聚酯纳米复合材料,其具有不同的组合物,0,0,0.5,1,1.5和2wt%CloisiteL5a为纳米填充物。 。研究了纳米粘土含量对纳米复合材料的机械,动态机械和热性能的影响。采用拉伸检测,冲击试验,动态力学分析和热重分析来研究机械和热特性。拉伸和冲击试验结果指向粘土负荷的最佳百分比为1%。拉伸模量也达到了针对不同的交叉头速度(CHS)填充的样品的最佳状态。动态机械行为并不表示任何一致的行为。然而,储存量度显示出1%纳米填充样品的改进性能。对于所有样品,玻璃化转变温度,T_G落在95至110℃的范围内。热重分析表明所有样品的第一阶段开始约200°C。通过扫描电子显微镜(SEM)分析的裂缝表面表示用玻璃纤维垫加强纯聚酯骨折的脆性性质,而通过添加纳米粘土,骨折变为延展性。

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