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Cell Structure Control of Porous Titanium Composite Synthesized by Combustion Reaction

机译:燃烧反应合成多孔钛复合材料的细胞结构控制

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Porous titanium matrix composites were fabricated by a reaction between titanium powder and boron carbide powder (B4C). Precursors were made by compacting the starting powder blend, and heated in an induction furnace to induce the reaction. The reaction was strongly exothermic and, therefore, it was a combustion mode when Ti/B_4C blending ratio of the starting powder was appropriate. The reaction product was both titanium boride (TiB or TiB_2) and titanium carbide (TiC). By controlling the Ti/B_4C blending ratio, it was possible to control the volume fraction of reaction products in titanium matrix. The combustion synthesized material was porous and its porous structure was strongly affected by the processing condition of the precursor (porosity of the precursor and 'Ti/B_4C blending ratio). The cell-edge size was varied from several tens of microns to about 500 microns by changing the combustion temperature.
机译:通过钛粉末和碳化硼粉(B4C)之间的反应来制造多孔钛基复合材料。通过压实起始粉末混合物制备前体,并在感应炉中加热以诱导反应。反应强烈放热,因此,当起始粉末的Ti / B_4C混合比合适时,它是一种燃烧模式。反应产物是硼化钛(Tib或Tib_2)和碳化钛(TiC)。通过控制Ti / B_4C混合比,可以控制钛基质中反应产物的体积分数。燃烧合成材料是多孔的,其多孔结构受到前体的加工条件的强烈影响(前体的孔隙率和'Ti / B_4C混合比)。通过改变燃烧温度,电池边缘尺寸从几十微米到约500微米的变化。

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