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MICROSTRUCTURAL ANALYSIS OF NUCLEAR GRADE GRAPHITE MATERIALS

机译:核级石墨材料的微观结构分析

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Graphite materials under nuclear services undergo very significant irradiation effects including dimensional instability and modifications in various thermo- physical and mechanical properties'1'4'. Because these changes are resulting from the irradiation-induced structural changes the graphite in nano-, micro- and meso-scopic scales, it is essential to adequately characterize the materials' structures before and after neutron irradiation and to correlate the structural changes with the evolving macroscopic properties. Objective of this work is to characterize the microstructures of the as-fabricate fine-grained nuclear graphite manufactured by Tokai Carbon Co., Ltd. The graphite consists of filler cokes, binder, pores, and inherent cracks. The characteristic microstructures of the fine-grained isotropic graphite were determined by focusing on the attributes of these elements. Specifically, the sizes, shape factors, and the crystallographic anisotropy were evaluated so that these properties may be correlated with the thermophysical properties, macroscopic anisotropy, fracture properties, and the irradiation effects on them. In future work, these materials will be examined for various properties and microstructural changes by the neutron irradiation in the High Flux Isotope Reactor, Oak Ridge National Laboratory. This paper gives the initial results of microstructural evaluation for the pre-irradiated materials.
机译:核服务下的石墨材料非常显着的辐照效应,包括各种热物理和机械性能的尺寸不稳定和修改1'4'。因为这些变化是由辐射诱导的结构改变纳米,微型和中学尺度的石墨,所以必须充分表征中子辐射前后的材料结构,并与发展的结构变化相关联宏观性质。这项工作的目的是表征由Tokai Cars Co.,Ltd。制造的AS制造的微粒核石墨的微观结构石墨包括填料焦炭,粘合剂,毛孔和固有裂缝。通过聚焦对这些元素的属性来确定细粒度各向同性石墨的特征微观结构。具体地,评估尺寸,形状因子和结晶各向异性,使得这些性质可以与热物理性质,宏观各向异性,裂缝性能和辐照效应相关。在未来的工作中,通过高通量同位素反应器,橡树岭国家实验室中中子辐射进行各种性能和微观结构变化的各种性质和微观结构变化。本文为预辐射材料提供了微观结构评价的初始结果。

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