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Preparation of Dense Al_2O_3 Film on 8YSZ Coating by Sol-Gel Method

机译:溶胶 - 凝胶法制备致密Al_2O_3薄膜的胶片

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The 8 wt.% yttria-stabilized zirconia (8YSZ) thermal barrier coatings (TBCs) are widely used to protect hot superalloy components of gas turbine and jet engine. However, Cracks and pores in the 8YSZ coating would accelerate the oxidation of the bondcoat alloy and the corrosion of 8YSZ topcoat by molten salts and finally result in permanent failure of the TBCs. Hence, in this work, a sol-gel spin-coating method was employed to prepare a densea-Al_2O_3 film on the surface of air-plasma-sprayed 8YSZ coatings, in order to block the paths of cracks and pores while keeping the stress tolerance of 8YSZ coatings.The influences of the polyvinylpyrrolidone (PVP) and alumina content of the sol on the microstructure of the α-Al_2O_3 film were investigated. It is found that a sol with PVP addition amount of50mg/mL and alumina solid contentof 10%let to the achievement of a compact α-Al_2O_3 film. The positive results in this work would inspire more efforts to prepare dense films on TBCs and therefore improve their performance under service conditions.
机译:8重量%。%yTTRIA稳定的氧化锆(8YSZ)热阻挡涂层(TBCS)广泛用于保护燃气轮机和喷射发动机的热超合金组分。然而,8苏斯涂层中的裂缝和孔将加速粘合剂合金的氧化和通过熔盐的腐蚀腐蚀,最后导致TBC的永久性失效。因此,在这项工作中,使用溶胶 - 凝胶旋涂方法在空气等离子体喷涂的8苏斯涂层表面上制备致密部分-Al_2O_3膜,以阻止裂缝和孔径的同时保持应力耐受性研究了80Sz涂层。研究了聚乙烯吡咯烷酮(PVP)和溶胶氧化铝含量对α-Al_2O_3膜的微观结构的影响。据发现,用PVP添加量of50mg / mL和氧化铝固体contentof 10%的溶胶让到一个紧凑的α-Al_2O_3的膜的实现。这项工作的积极成果将激发更多的努力在TBC上制备密集的薄膜,从而改善其在服务条件下的性能。

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