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INVESTIGATION OF THE COEXTRUSION FLOW STABILITY IN FLAT DIES FOR DIFFERENT BATCHES OF THE SAME POLYMER

机译:不同批次扁平模具中共挤出流动稳定性的研究

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The work presents both, simulation and experimental findings of the research of two LDPE melts using a flat coextrusion flow visualization cell. The simulation is performed by FEM analysis with full u-v-p-τ numerical scheme employing viscoelastic constitutive equations. The predicted stresses, velocities and interface location have been found to be in a good agreement with the measurements. The experimental analysis shows that pronounced wave instabilities are caused by the minor layer break at the merge point of the layers, and extensional viscosity is a driving parameter here. A recently proposed ‘TNSD sign criterion’ (Zatloukal et al, Int Polym Proc., 16(2) 198-207 2001), which quantifies the relative stretching of the layers in the merging area has been successfully tested for the prediction of the onset of wave interfacial instabilities in this type of the die geometry. Moreover, rheological and molecular characteristics (MWD) were experimentally determined for different batches of LDPE. The results show that extensional viscosity may significantly vary for different batches even if shear viscosities and MWDs are very similar. FEM analysis together with TNSD value calculation was consequently performed to determine the stability of the coextrusion flow in the flat die for different batches of the material and the effect was found considerable.
机译:该工作介绍了使用扁平共挤出流动可视化细胞的两个LDPE熔融研究的模拟和实验结果。用采用粘弹性本构剖面方程的全U-V-P-τ数值方案进行了有限元分析来执行模拟。已经发现预测的应力,速度和接口位置与测量有关。实验分析表明,明显的波形不稳定性是由层的合并点处的次要层断裂引起的,并且延伸粘度是这里的驱动参数。最近提出的“TNSD符号标准”(Zatloukal等,INT Polum Proc。,16(2)198-207 2001),其定量了合并区域中的层中的层相对拉伸,以预测发作的预测这种基芯几何中的波界面不稳定性。此外,针对不同批次的LDPE实验确定流变和分子特性(MWD)。结果表明,即使剪切粘度和MWDS非常相似,延伸粘度也可能显着变化。因此,对TNSD值计算的有限分析进行了与TNSD值计算一起以确定用于不同批次的平坦模具中的共挤出流动的稳定性,并且发现效果很大。

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