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INVESTIGATION OF THE COEXTRUSION FLOW STABILITY IN FLAT DIES FOR DIFFERENT BATCHES OF THE SAME POLYMER

机译:同一聚合物不同批次的平板模具中共挤出流动稳定性的研究

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The work presents both, simulation and experimental findings of the research of two LDPE melts using a flatcoextrusion flow visualization cell. The simulation is performed by FEM analysis with full u-v-p-τ numerical schemeemploying viscoelastic constitutive equations. The predicted stresses, velocities and interface location have been foundto be in a good agreement with the measurements. The experimental analysis shows that pronounced wave instabilitiesare caused by the minor layer break at the merge point of the layers, and extensional viscosity is a driving parameterhere. A recently proposed ‘TNSD sign criterion’ (Zatloukal et al, Int Polym Proc., 16(2) 198-207 2001), whichquantifies the relative stretching of the layers in the merging area has been successfully tested for the prediction of theonset of wave interfacial instabilities in this type of the die geometry. Moreover, rheological and molecularcharacteristics (MWD) were experimentally determined for different batches of LDPE. The results show thatextensional viscosity may significantly vary for different batches even if shear viscosities and MWDs are very similar.FEM analysis together with TNSD value calculation was consequently performed to determine the stability of thecoextrusion flow in the flat die for different batches of the material and the effect was found considerable.
机译:该工作介绍了使用平整机对两种LDPE熔体进行研究的模拟结果和实验结果。 共挤流动可视化单元。通过具有完整u-v-p-τ数值方案的FEM分析进行仿真 使用粘弹性本构方程。发现了预计的应力,速度和界面位置 与测量值保持良好的一致性实验分析表明,明显的波不稳定性 是由于在层的合并点处的较小的层破裂而引起的,而拉伸粘度是驱动参数 这里。最近提出的“ TNSD标志标准”(Zatloukal等人,Int Polym Proc。,16(2)198-207 2001),其中 量化合并区域中各层的相对拉伸已成功测试以预测 这种类型的模具几何形状中波界面不稳定性的开始。此外,流变学和分子学 通过实验确定了不同批次的LDPE的特性(MWD)。结果表明 即使剪切粘度和MWD非常相似,对于不同的批次,拉伸粘度也可能发生显着变化。 因此,进行了有限元分析和TNSD值计算,从而确定了稳定性。 对于不同批次的材料,在平模中共挤出流动,并且发现效果显着。

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