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Structure investigations of low-temperature MBE grown InAlAs layers on InP001 substrate

机译:InP 001衬底上低温MBE生长的InAlAs层的结构研究

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The real crystal structure of In/sub 0.52/AI/sub 0.48/As layers grown on InP>001< substrate as a function of the growth temperature (between 150/spl deg/C and 450/spl deg/C) was investigated. Both as-grown and annealed samples (500/spl deg/C) show a high electrical resistivity (10/sup 6-10/sup 7//spl Omega/cm). The following structural /electrical analyses were applied to these samples: transmission electron microscopy (TEM), x-ray diffraction, particle induced x-ray emission (PIXE). In the temperature range between 200/spl deg/C and 450/spl deg/C good crystalline InAlAs layers can be achieved with a low density of dislocations and stacking faults. A generation of precipitates as in the case of LT-GaAs could not be observed. Furthermore, ordering of group-III elements on {111} planes was observed in these layers. Structure models of such ordered domains are discussed. At growth temperatures below 300/spl deg/C additional As (/spl ap/1-2%) is incorporated in the lattice. For layers grown below 200/spl deg/C "pyramidal defects" are formed containing small inclusions of hexagonal As precipitates in the core of these defects.
机译:研究了在InP> 001 <衬底上生长的In / sub 0.52 / Al / sub 0.48 / As层的实际晶体结构与生长温度(在150 / spl deg / C和450 / spl deg / C之间)的关系。生长和退火的样品(500 / spl deg / C)都显示出高电阻率(10 / sup 6-10 / sup 7 // splΩ/ cm)。将以下结构/电分析应用于这些样品:透射电子显微镜(TEM),X射线衍射,粒子诱导X射线发射(PIXE)。在200 / spl deg / C和450 / spl deg / C之间的温度范围内,可以以低的位错密度和堆垛层错获得良好的晶体InAlAs层。如在LT-GaAs的情况下,未观察到沉淀的产生。此外,在这些层中观察到III族元素在{111}平面上的排序。讨论了这种有序域的结构模型。在低于300 / spl deg / C的生长温度下,将额外的As(/ spl ap / 1-2%)掺入晶格中。对于生长在200 / spl deg / C以下的层,会形成“金字塔形缺陷”,在这些缺陷的核心中包含少量的六方晶系As沉淀物。

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