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NAMS/ICIM 2010, Washington D.C., USA

机译:NAMS / ICIM 2010,美国华盛顿特区

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摘要

ZIF-8 membranes were synthesized by in-situ crystallization on tubular porous α-alumina supports.First, ZIF-8 seeds were prepared solvothermally from a solution containing zinc nitrate hexahydrate, methanol, and 2-methylimidazole. This solution was transferred to a teflon lined stainless steel autoclave and heated in a conventional oven at 150℃ for 5 hrs. After cooling, the solids were separated by centrifugation and washed with methanol.
机译:ZIF-8膜是通过在管状多孔α-氧化铝载体上原位结晶而合成的。首先,从含有六水合硝酸锌,甲醇和2-甲基咪唑的溶液中溶剂热制备ZIF-8晶种。将该溶液转移至衬有特氟隆的不锈钢高压釜中,并在常规烘箱中于150℃加热5小时。冷却后,通过离心分离固体,并用甲醇洗涤。

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