首页> 外国专利> SPECIAL PIG MANURE CHARCOAL MODIFIED BY AMINO GRAFTING, PREPARATION METHOD, AND USE THEREOF IN FARMLAND WATER-REMOVING AND NITROGEN RECYCLING

SPECIAL PIG MANURE CHARCOAL MODIFIED BY AMINO GRAFTING, PREPARATION METHOD, AND USE THEREOF IN FARMLAND WATER-REMOVING AND NITROGEN RECYCLING

机译:特种猪粪木炭通过氨基嫁接,制备方法和氮气再循环中的制备方法和使用

摘要

The present invention relates to a preparation method for a carbon-based fertilizer, and in particular, to special pig manure charcoal modified by amino grafting, a preparation method, and use thereof in farmland water-removing and nitrogen recycling. A preparation method for special pig manure charcoal modified by amino grafting. The method comprises the following steps: 1. drying raw materials: dehydrating the raw material pig manure to a water content of 80%-85%, and then successively performing acid washing, drying, and crushing to obtain dry pig manure powder; (2) performing liquid nitrogen pretreatment and high temperature carbonization to obtain expanded pig manure charcoal; (3) performing carboxylation treatment to obtain carboxylated pig manure charcoal; and (4) grafting amino groups: adding the carboxylated pig manure charcoal prepared in step 3 into an aqueous ammonia fluid, stirring for 20-24 h under heating conditions of an oil bath at 200-240 °C, cooling to room temperature, then washing and filtering the reaction product, blowing same with N2, drying the product in vacuum at 110±5 °C for 12-24 h, and grinding same, so as to obtain special pig manure charcoal modified by amino grafting.
机译:本发明涉及碳肥料的制备方法,特别涉及通过氨基接枝,制备方法和氮回收中的氨基嫁接,制备方法和使用中的特殊猪粪木炭。氨基嫁接改性特殊猪粪木炭的制备方法。该方法包括以下步骤:1。干燥原料:将原料猪粪脱水至80%-85%的水含量,然后连续进行酸洗,干燥和压碎以获得干猪粪粉; (2)进行液氮预处理和高温碳化,得到膨胀猪粪木炭; (3)进行羧化处理,得到羧化猪粪炭; (4)嫁接氨基:将步骤3中制备的羧化猪粪炭加入氨水中,在200-240℃的油浴的加热条件下搅拌20-24小时,冷却至室温,然后洗涤和过滤反应产物,与N 2相同,将产物在110±5℃下真空干燥12-24小时,并磨削相同,从而获得通过氨基接枝改性的特殊猪粪木炭。

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