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TITANIUM-CONTAINING CALCIUM HEXALUMINATE MATERIAL AND PREPARATION METHOD THEREFOR

机译:含钛的六铝酸钙材料及其制备方法

摘要

A titanium-containing calcium hexaluminate material and a preparation method therefor. The technical solution is: using as raw material 60-80 wt% aluminum oxide micro powder, 5-20wt% calcium-containing micro powder, 10-20wt% titanium oxide micro powder, and 1-10wt% manganous oxide micro powder, uniformly mixing the raw material in a planetary ball mill to obtain a mixture; then molding the mixture by means of mechanical pressing at 100-200 MPa to obtain a green body; and drying the green body at 110-200˚C for 12-36 hours, and carrying out heat preservation at 1500-1800˚C for 1-8 hours to obtain the titanium-containing calcium hexaluminate material. The particle size D50 of the aluminum oxide micro powder is 1-8 μm; the particle size D50 of the calcium-containing micro powder is 1-10 μm; the particle size D50 of the titanium oxide micro powder is 1-10 μm; the particle size D50 of the manganous oxide micro powder is 1-8 μm. The preparation method is low in cost and involves a simple process. The prepared product has good chemical stability, good thermal shock resistance, and strong titanium-aluminum alloy melt resistance.
机译:含钛氧化钙六铝材料及其制备方法。技术方案是:用作原料60-80wt%铝氧化物微粉,5-20wt%含钙的微粉,10-20wt%氧化钛微粉,1-10wt%氧化锰微粉,均匀混合行星球磨机中的原料以获得混合物;然后通过在100-200MPa的机械压制下模塑混合物以获得生坯;并在110-200℃下干燥绿体12-36小时,并在1500-1800℃下进行保温1-8小时,得到含钛六氢材料。氧化铝微粉的粒径D50为1-8μm;含钙的微粉的粒径D50为1-10μm;氧化钛微粉的粒径D50为1-10μm;氧化锰微粉的粒径D50为1-8μm。制备方法成本低,涉及简单的过程。制备的产品具有良好的化学稳定性,良好的耐热抗冲击性和强钛 - 铝合金熔体抗性。

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