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Method for producing a single crystal

机译:制造单晶的方法

摘要

A method for producing a single crystal from a crude melt contained in a quartz crucible placed in a furnace of an apparatus for producing a single crystal according to a Czochralski method, comprising: examining in advance a correlation between a molar concentration ratio of Al to Li, contained in a quartz raw material powder used for manufacturing the quartz crucible, a usage time of the quartz crucible, a ratio of a thickness of a devitrification part to a thickness of the quartz crucible at the time of use, and occurrence or non-occurrence of melt leakage attributable to the devitrification part; setting a range the ratio of the thickness of the devitrification part to the thickness of the quartz crucible used for growing the single crystal so as not to generate any melt leakage attributable to the devitrification part; and determining a maximum usage time for the quartz crucible gel according to the molar concentration ratio of Al to Li contained in the quartz raw material powder used for manufacturing the quartz crucible so as to fall within the set range of the ratio based on the correlation; and growing the single crystal using the quartz crucible in the range of the maximum use time.
机译:一种从包含在石英坩埚中含有的粗熔体的单晶制备单晶的方法,该方法放置在根据Czochralski方法的制造单晶的装置的炉中,包括:预先检查Al到Li的摩尔浓度比之间的相关性,包含在用于制造石英坩埚的石英原料粉末中,使用石英坩埚的使用时间,在使用时的石英坩埚的厚度的厚度的厚度的比率,以及发生或非贫困部分可归因于缺失部分的熔体泄漏;设定偏差部分的厚度与用于生长单晶的石英坩埚的厚度的范围,以免产生可归因于缺失部分的任何熔体泄漏;根据用于制造石英坩埚的石英原材料粉末中包含的摩尔浓度比,根据用于制造石英坩埚中的摩尔浓度比,确定石英坩埚凝胶的最大用途时间,以基于相关性的比率的设定范围内;并使用石英坩埚在最大使用时间范围内生长单晶。

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