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metallic naonoparticle bound to the surface of mesoporous silica support having ordered 3-D pore structure and method for preparation thereof

机译:与介孔二氧化硅载体表面有序的3-D孔结构的金属去氨基粒子,其制备方法及其制备方法

摘要

The present invention includes the steps of: (a) introducing multiple amine groups on the surface of the mesoporous silica support having an ordered three-dimensional pore structure; (b) introducing metal ions by contacting the mesoporous silica support having a regular three-dimensional pore structure in which the multiple amine groups are immobilized with an active metal precursor; And (c) reducing the adsorbed metal ions to form metal nanoparticles, comprising a mesoporous silica support having a regular three-dimensional pore structure, and metal nanoparticles fixed to the inner and outer surfaces of the pores thereof. It relates to a method of manufacturing a composite containing and metal nanoparticles fixed on a mesoporous silica support having a three-dimensional pore structure thus prepared, the process is simplified, and the surface area is increased by the use of a silica support having a three-dimensional shape. , It can be applied as a heterogeneous catalyst.
机译:本发明包括以下步骤:(a)在具有有序的三维孔结构的中孔二氧化硅载体的表面上引入多个胺基; (b)通过接触具有常规三维孔结构的介孔二氧化硅载体引入金属离子,其中多个胺基通过活性金属前体固定; (c)减少吸附金属离子以形成金属纳米颗粒,其包含具有常规三维孔结构的介孔二氧化硅载体,以及固定在其孔的内表面和外表面的金属纳米颗粒。它涉及一种制造固定在具有三维孔结构的中孔二氧化硅载体上的复合材料和金属纳米颗粒的方法,简化了该方法,通过使用具有三个二氧化硅载体来增加表面积。 - 形状。 ,它可以作为异质催化剂施用。

著录项

  • 公开/公告号KR102224575B1

    专利类型

  • 公开/公告日2021-03-09

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR1020190083788

  • 发明设计人 조병기;이영민;

    申请日2019-07-11

  • 分类号B01J37;B01J21/08;B01J23/42;B01J23/44;B01J35/02;B01J35/10;B01J37/16;C01B15/01;

  • 国家 KR

  • 入库时间 2022-08-24 17:35:04

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