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Environmental water analytical instrument

机译:环境水质分析仪

摘要

PURPOSE:To make sepn. with every component with high resolving power by passing a gas contg. an objective component through a porous polystyrene prior to an analysis, enriching only the volatile component selectively at a high ratio and injecting the same into a capillary column. CONSTITUTION:A flow passage to a carrier gas source 4 inflow port 2b of an aeration vessel a sample enricher 1a a port 6 open to the atm. is first formed. The carrier gas is admitted into the aeration vessel 2, then the volatile component contained in a sample (S) is separated and is conveyed together with the carrier gas to the enricher 1 where the volatile component is adsorbed to an adsorbent 1b packed in the enricher 1 and the sample is enriched. A flow passage to the gas source 4 the enricher 1 the sample inlt port 7 a sample injection mechanism 8 the capillary column 9 is then formed, and a capillary tube 9a of the mechanism 8 is immersed in a liquefied gas tank 8b, by which said tube is cooled to a cryogenic temp. While the carrier gas is passed to the enricher 1, a heater 1d is electrically heated. The adsorbed 1b volatile component is then condensed together with the carrier gas in the tube 9a and is separated to every component by the high resolving power of the column 9.
机译:目的:做septn。通过气体控制,使每个组件具有较高的分辨能力。在分析之前先通过多孔聚苯乙烯形成目标组分,然后仅以高比例选择性富集挥发性组分,然后将其注入毛细管柱。组成:通向曝气容器载气源4入口2b的流道,样品浓缩器1a和通向大气压的端口6。首先形成。将载气送入曝气容器2中,然后分离样品(S)中所含的挥发性成分,并与载气一起输送至富集器1,在该富集器1中,该挥发性成分被吸附至填充在富集器中的吸附剂1b上。 1,样品富集。然后形成通向气体源4,富集器1,样品注入口7,样品注入机构8,毛细管柱9的流动通道,并且将机构8的毛细管9a浸入液化气罐8b中,通过所述液化气罐8b将管冷却至低温。当载气通过浓缩器1时,加热器1d被电加热。然后,被吸附的1b挥发性成分与载气一起在管9a中冷凝,并通过塔9的高分离能力被分离成每种成分。

著录项

  • 公开/公告号JP2588168B2

    专利类型

  • 公开/公告日1997-03-05

    原文格式PDF

  • 申请/专利权人 株式会社島津製作所;

    申请/专利号JP19860029486

  • 发明设计人 松居 正己;

    申请日1986-02-12

  • 分类号G01N33/18;B01D15/08;G01N30/08;G01N30/16;

  • 国家 JP

  • 入库时间 2022-08-22 03:28:15

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