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Plasma Torch Cleaning Method of Inductively Coupled Plasma Emission Spectrometer

机译:电感耦合等离子体发射光谱仪的等离子炬清洗方法

摘要

The present invention relates to a method for cleaning a plasma torch of an inductively coupled plasma light emitting spectrometer for elemental analysis, by maximizing the cleaning power of the torch by using a cleaning solution having excellent solubility in a composite oxide containing carbon attached to the torch. The purpose of the present invention is to provide an excellent cleaning method that can maximize the work efficiency by not only smoothing the generation of smear but also preventing the high frequency work coil damage and work safety caused by the extension of the torch and electrical short circuit.;The present invention provides a method for cleaning a plasma torch of an inductively coupled plasma light spectrometer, including acetone: 100-200 ml / l, hydrochloric acid: 200-300 ml / l, sulfuric acid: 500-700 ml / l, and potassium dichromate: Preparing a cleaning liquid that is formulated at 30-40 g / l; Immersing the plasma torch to be cleaned in the cleaning solution prepared as described above, heating the cleaning solution to 50-80 ° C., and maintaining the temperature at the temperature for 1-2 hours to perform the first cleaning; Second cleaning by dipping the first cleaned plasma torch in acetone as described above; Rinsing the ultra pure distilled water with the secondary cleaned plasma torch as described above; And a plasma torch cleaning method of an inductively coupled plasma light spectrometer comprising the step of drying the rinsed plasma torch for 30-60 minutes at 90-100 ° C.
机译:本发明涉及一种用于清洁元素分析的电感耦合等离子体发光光谱仪的等离子体炬的方法,该方法是通过使用在附着于该炬的含碳复合氧化物中具有优异溶解性的清洗液来最大化炬的清洗能力。 。发明内容本发明的目的是提供一种优异的清洁方法,该方法不仅可以平滑拖尾的产生,而且还可以防止由于割炬的延伸和短路引起的高频工作线圈损坏和工作安全性,从而使工作效率最大化。本发明提供了一种清洁感应耦合等离子体光谱仪的等离子体炬的方法,包括丙酮:100-200ml / l,盐酸:200-300ml / l,硫酸:500-700ml / l ,以及重铬酸钾:配制30-40 g / l的清洁液;将待清洗的等离子炬浸入如上所述制备的清洗液中,将清洗液加热至50-80℃,并在该温度下保持1-2小时以进行第一次清洗;如上所述,通过将第一清洁的等离子体炬浸入丙酮中进行第二清洁;如上所述,用二次清洁的等离子炬冲洗超纯蒸馏水;以及感应耦合等离子体光谱仪的等离子炬清洁方法,其包括以下步骤:在90-100℃下将冲洗后的等离子炬干燥30-60分钟。

著录项

  • 公开/公告号KR19980043980A

    专利类型

  • 公开/公告日1998-09-05

    原文格式PDF

  • 申请/专利权人 김종진;

    申请/专利号KR19960061971

  • 发明设计人 허운;

    申请日1996-12-05

  • 分类号B08B3/00;

  • 国家 KR

  • 入库时间 2022-08-22 02:48:12

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